(E)-methyl 4-(2-((E)-(3-bromofuran-2-yl)methyleneamino)-2,2-diphenylacetoxy)but-2-enoate

Base Information

Chemical Name:(E)-methyl 4-(2-((E)-(3-bromofuran-2-yl)methyleneamino)-2,2-diphenylacetoxy)but-2-enoate
CAS No.:1086429-78-8
Molecular Formula:C₂₄H₂₀BrNO₅
Molecular Weight:482.331
Hs Code.:

Synonyms:(E)-methyl 4-(2-((E)-(3-bromofuran-2-yl)methyleneamino)-2,2-diphenylacetoxy)but-2-enoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-methyl 4-(2-((E)-(3-bromofuran-2-yl)methyleneamino)-2,2-diphenylacetoxy)but-2-enoate

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Technology Process of (E)-methyl 4-(2-((E)-(3-bromofuran-2-yl)methyleneamino)-2,2-diphenylacetoxy)but-2-enoate

There total 1 articles about (E)-methyl 4-(2-((E)-(3-bromofuran-2-yl)methyleneamino)-2,2-diphenylacetoxy)but-2-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 14757-78-9
3-bromofurfural

: 1086429-92-6
C₁₉H₁₉NO₄

: 1086429-78-8
(E)-methyl 4-(2-((E)-(3-bromofuran-2-yl)methyleneamino)-2,2-diphenylacetoxy)but-2-enoate

Guidance literature:: In benzene; Reflux; Inert atmosphere;
DOI:10.1021/ol801986m

Reference yield: 88.0%

: 1086429-78-8
(E)-methyl 4-(2-((E)-(3-bromofuran-2-yl)methyleneamino)-2,2-diphenylacetoxy)but-2-enoate

: 1086429-82-4
(E)-methyl 2-(6-(diphenylmethyleneamino)-5,6-dihydro-4H-cyclopenta[b]furan-4-ylidene)acetate

Guidance literature:: (E)-methyl 4-(2-((E)-(3-bromofuran-2-yl)methyleneamino)-2,2-diphenylacetoxy)but-2-enoate; With tetrakis(triphenylphosphine) palladium⁽⁰⁾; silver sulfate; In N,N-dimethyl-formamide; at 20 ℃; for 0.25h; Inert atmosphere;

With triethylamine; In N,N-dimethyl-formamide; at 150 ℃; for 0.5h; Inert atmosphere; Microwave irradiation;
DOI:10.1021/ol801986m