6,9,12,15,18-pentamethyl-43,46,49,52,55-pentaphenyl-1,6,9,12,15,18,43,46,49,52,55,56-dodecahydro(C⁶⁰-I^h)[5,6]fullerene

Base Information

• Chemical Name: 6,9,12,15,18-pentamethyl-43,46,49,52,55-pentaphenyl-1,6,9,12,15,18,43,46,49,52,55,56-dodecahydro(C⁶⁰-I^h)[5,6]fullerene
• CAS No.: 503835-63-0
• Molecular Formula: C₉₅H₄₂
• Molecular Weight: 1183.38

Synonyms:6,9,12,15,18-pentamethyl-43,46,49,52,55-pentaphenyl-1,6,9,12,15,18,43,46,49,52,55,56-dodecahydro(C⁶⁰-I^h)[5,6]fullerene

Chemical Property of 6,9,12,15,18-pentamethyl-43,46,49,52,55-pentaphenyl-1,6,9,12,15,18,43,46,49,52,55,56-dodecahydro(C⁶⁰-I^h)[5,6]fullerene

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Technology Process of 6,9,12,15,18-pentamethyl-43,46,49,52,55-pentaphenyl-1,6,9,12,15,18,43,46,49,52,55,56-dodecahydro(C⁶⁰-I^h)[5,6]fullerene

There total 1 articles about 6,9,12,15,18-pentamethyl-43,46,49,52,55-pentaphenyl-1,6,9,12,15,18,43,46,49,52,55,56-dodecahydro(C⁶⁰-I^h)[5,6]fullerene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-cyano-6,9,12,15,18-pentamethyl-43,46,49,52,55-pentaphenyl-1,6,9,12,15,18,43,46,49,52,55,56-dodecahydro(C60-Ih)[5,6]fullerene (503835-64-1) → 6,9,12,15,18-pentamethyl-43,46,49,52,55-pentaphenyl-1,6,9,12,15,18,43,46,49,52,55,57-dodecahydro(C60-Ih)[5,6]fullerene (745075-55-2) + 6,9,12,15,18-pentamethyl-43,46,49,52,55-pentaphenyl-1,6,9,12,15,18,43,46,49,52,55,60-dodecahydro(C60-Ih)[5,6]fullerene + 6,9,12,15,18-pentamethyl-43,46,49,52,55-pentaphenyl-1,6,9,12,15,18,43,46,49,52,55,56-dodecahydro(C60-Ih)[5,6]fullerene (503835-63-0)

Guidance literature:

With naphthalen-1-yl-lithium; In tetrahydrofuran; benzonitrile; at 23 ℃; for 1h; Title compound not separated from byproducts.;

DOI:10.1021/ja029915z

Reference yield: 42.0%

6,9,12,15,18-pentamethyl-43,46,49,52,55-pentaphenyl-1,6,9,12,15,18,43,46,49,52,55,56-dodecahydro(C60-Ih)[5,6]fullerene (503835-63-0) → C95H42O5

Guidance literature:

6,9,12,15,18-pentamethyl-43,46,49,52,55-pentaphenyl-1,6,9,12,15,18,43,46,49,52,55,56-dodecahydro(C⁶⁰-I^h)[5,6]fullerene; With potassium hydride; In tetrahydrofuran;

With air; In tetrahydrofuran; Further stages.;

DOI:10.1021/ja029915z

Reference yield: 26.0%

cyclopentadienyl iron(II) dicarbonyl dimer (38117-54-3) + 6,9,12,15,18-pentamethyl-43,46,49,52,55-pentaphenyl-1,6,9,12,15,18,43,46,49,52,55,56-dodecahydro(C60-Ih)[5,6]fullerene (503835-63-0) → (C5H5)2Fe2(C60(CH3)5(C6H5)5)

Guidance literature:

In benzonitrile; cyclophenacene compd. treated with Fe complex (5 equiv.) in PhCN at 185°C; detd. by (1)H and (13)C NMR and mass spectra;

DOI:10.1021/ja061175x

upstream raw materials:

1-cyano-6,9,12,15,18-pentamethyl-43,46,49,52,55-pentaphenyl-1,6,9,12,15,18,43,46,49,52,55,56-dodecahydro(C⁶⁰-I^h)[5,6]fullerene

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