(1S,2S,3S,4R,5R)-4-[2-(4-Methoxy-phenoxy)-ethyl]-2-propyl-6,8-dioxa-bicyclo[3.2.1]octan-3-ol

Base Information

Chemical Name:(1S,2S,3S,4R,5R)-4-[2-(4-Methoxy-phenoxy)-ethyl]-2-propyl-6,8-dioxa-bicyclo[3.2.1]octan-3-ol
CAS No.:157117-00-5
Molecular Formula:C₁₈H₂₆O₅
Molecular Weight:322.401
Hs Code.:

Synonyms:(1S,2S,3S,4R,5R)-4-[2-(4-Methoxy-phenoxy)-ethyl]-2-propyl-6,8-dioxa-bicyclo[3.2.1]octan-3-ol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1S,2S,3S,4R,5R)-4-[2-(4-Methoxy-phenoxy)-ethyl]-2-propyl-6,8-dioxa-bicyclo[3.2.1]octan-3-ol

Chemical Property:

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Technology Process of (1S,2S,3S,4R,5R)-4-[2-(4-Methoxy-phenoxy)-ethyl]-2-propyl-6,8-dioxa-bicyclo[3.2.1]octan-3-ol

There total 8 articles about (1S,2S,3S,4R,5R)-4-[2-(4-Methoxy-phenoxy)-ethyl]-2-propyl-6,8-dioxa-bicyclo[3.2.1]octan-3-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (1S,2S,3S,4R,5R)-2-Allyl-4-[2-(4-methoxy-phenoxy)-ethyl]-6,8-dioxa-bicyclo[3.2.1]octan-3-ol

: 157117-00-5
(1S,2S,3S,4R,5R)-4-[2-(4-Methoxy-phenoxy)-ethyl]-2-propyl-6,8-dioxa-bicyclo[3.2.1]octan-3-ol

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; Yield given;
DOI:10.1016/S0040-4039(00)75797-2

Reference yield:

: 33208-47-8
4-O-benzyl-1,6:2,3-dianhydro-β-D-mannopyranose

: 157117-00-5
(1S,2S,3S,4R,5R)-4-[2-(4-Methoxy-phenoxy)-ethyl]-2-propyl-6,8-dioxa-bicyclo[3.2.1]octan-3-ol

Guidance literature:: Multi-step reaction with 9 steps

1: diethyl ether / Ambient temperature

2: Et₃N / DMAP / CH₂Cl₂ / Ambient temperature

4: DEAD-Ph₃P / CH₂Cl₂ / Ambient temperature

5: H₂ / Pd/C / methanol

6: Et₃N / CH₂Cl₂ / -10 °C

7: MeONa / methanol / Ambient temperature

8: diethyl ether / Ambient temperature

9: H₂ / Pd/C / methanol

With hydrogen; sodium methylate; triethylamine; triphenylphosphine; diethylazodicarboxylate; dmap; palladium on activated charcoal; In methanol; diethyl ether; dichloromethane;
DOI:10.1016/S0040-4039(00)75797-2

Reference yield:

: 104206-19-1
1,6-anhydro-4-O-benzyl-2-deoxy-2-C-(2-propenyl)-β-D-glucopyranose

: 157117-00-5
(1S,2S,3S,4R,5R)-4-[2-(4-Methoxy-phenoxy)-ethyl]-2-propyl-6,8-dioxa-bicyclo[3.2.1]octan-3-ol

Guidance literature:: Multi-step reaction with 8 steps

1: Et₃N / DMAP / CH₂Cl₂ / Ambient temperature

3: DEAD-Ph₃P / CH₂Cl₂ / Ambient temperature

4: H₂ / Pd/C / methanol

5: Et₃N / CH₂Cl₂ / -10 °C

6: MeONa / methanol / Ambient temperature

7: diethyl ether / Ambient temperature

8: H₂ / Pd/C / methanol

With hydrogen; sodium methylate; triethylamine; triphenylphosphine; diethylazodicarboxylate; dmap; palladium on activated charcoal; In methanol; diethyl ether; dichloromethane;
DOI:10.1016/S0040-4039(00)75797-2