(2S,3S,4S,5R,6S)-2-(tert-Butyl-diphenyl-silanyloxymethyl)-6-methoxy-5-[2-(4-methoxy-phenoxy)-ethyl]-3-propyl-tetrahydro-pyran-4-ol

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Chemical Name:(2S,3S,4S,5R,6S)-2-(tert-Butyl-diphenyl-silanyloxymethyl)-6-methoxy-5-[2-(4-methoxy-phenoxy)-ethyl]-3-propyl-tetrahydro-pyran-4-ol
CAS No.:157117-01-6
Molecular Formula:C₃₅H₄₈O₆Si
Molecular Weight:592.848
Hs Code.:

Synonyms:(2S,3S,4S,5R,6S)-2-(tert-Butyl-diphenyl-silanyloxymethyl)-6-methoxy-5-[2-(4-methoxy-phenoxy)-ethyl]-3-propyl-tetrahydro-pyran-4-ol

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Chemical Property of (2S,3S,4S,5R,6S)-2-(tert-Butyl-diphenyl-silanyloxymethyl)-6-methoxy-5-[2-(4-methoxy-phenoxy)-ethyl]-3-propyl-tetrahydro-pyran-4-ol

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Technology Process of (2S,3S,4S,5R,6S)-2-(tert-Butyl-diphenyl-silanyloxymethyl)-6-methoxy-5-[2-(4-methoxy-phenoxy)-ethyl]-3-propyl-tetrahydro-pyran-4-ol

There total 11 articles about (2S,3S,4S,5R,6S)-2-(tert-Butyl-diphenyl-silanyloxymethyl)-6-methoxy-5-[2-(4-methoxy-phenoxy)-ethyl]-3-propyl-tetrahydro-pyran-4-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 33208-47-8
4-O-benzyl-1,6:2,3-dianhydro-β-D-mannopyranose

: 157117-01-6
(2S,3S,4S,5R,6S)-2-(tert-Butyl-diphenyl-silanyloxymethyl)-6-methoxy-5-[2-(4-methoxy-phenoxy)-ethyl]-3-propyl-tetrahydro-pyran-4-ol

Guidance literature:: Multi-step reaction with 11 steps

1: diethyl ether / Ambient temperature

2: Et₃N / DMAP / CH₂Cl₂ / Ambient temperature

4: DEAD-Ph₃P / CH₂Cl₂ / Ambient temperature

5: H₂ / Pd/C / methanol

6: Et₃N / CH₂Cl₂ / -10 °C

7: MeONa / methanol / Ambient temperature

8: diethyl ether / Ambient temperature

9: H₂ / Pd/C / methanol

10: H⁽¹⁺⁾

11: pyridine

With pyridine; hydrogen; sodium methylate; hydrogen cation; triethylamine; triphenylphosphine; diethylazodicarboxylate; dmap; palladium on activated charcoal; In methanol; diethyl ether; dichloromethane;
DOI:10.1016/S0040-4039(00)75797-2

Reference yield:

: 104206-19-1
1,6-anhydro-4-O-benzyl-2-deoxy-2-C-(2-propenyl)-β-D-glucopyranose

: 157117-01-6
(2S,3S,4S,5R,6S)-2-(tert-Butyl-diphenyl-silanyloxymethyl)-6-methoxy-5-[2-(4-methoxy-phenoxy)-ethyl]-3-propyl-tetrahydro-pyran-4-ol

Guidance literature:: Multi-step reaction with 10 steps

1: Et₃N / DMAP / CH₂Cl₂ / Ambient temperature

3: DEAD-Ph₃P / CH₂Cl₂ / Ambient temperature

4: H₂ / Pd/C / methanol

5: Et₃N / CH₂Cl₂ / -10 °C

6: MeONa / methanol / Ambient temperature

7: diethyl ether / Ambient temperature

8: H₂ / Pd/C / methanol

9: H⁽¹⁺⁾

10: pyridine

With pyridine; hydrogen; sodium methylate; hydrogen cation; triethylamine; triphenylphosphine; diethylazodicarboxylate; dmap; palladium on activated charcoal; In methanol; diethyl ether; dichloromethane;
DOI:10.1016/S0040-4039(00)75797-2

Reference yield:

: 157116-99-9
(1R,2R,4R,5R,6R)-5-[2-(4-Methoxy-phenoxy)-ethyl]-3,7,9-trioxa-tricyclo[4.2.1.0^2,4]nonane

: 157117-01-6
(2S,3S,4S,5R,6S)-2-(tert-Butyl-diphenyl-silanyloxymethyl)-6-methoxy-5-[2-(4-methoxy-phenoxy)-ethyl]-3-propyl-tetrahydro-pyran-4-ol

Guidance literature:: Multi-step reaction with 4 steps

1: diethyl ether / Ambient temperature

2: H₂ / Pd/C / methanol

3: H⁽¹⁺⁾

4: pyridine

With pyridine; hydrogen; hydrogen cation; palladium on activated charcoal; In methanol; diethyl ether;
DOI:10.1016/S0040-4039(00)75797-2