7,9-dimethyl-1-phenyl-2,3,4,5-tetrahydro-1H-pyrrolo[1,2-a][1,4]diazepine

Base Information

Chemical Name:7,9-dimethyl-1-phenyl-2,3,4,5-tetrahydro-1H-pyrrolo[1,2-a][1,4]diazepine
CAS No.:1030615-63-4
Molecular Formula:C₁₆H₂₀N₂
Molecular Weight:240.348
Hs Code.:

Synonyms:7,9-dimethyl-1-phenyl-2,3,4,5-tetrahydro-1H-pyrrolo[1,2-a][1,4]diazepine

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Chemical Property of 7,9-dimethyl-1-phenyl-2,3,4,5-tetrahydro-1H-pyrrolo[1,2-a][1,4]diazepine

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Technology Process of 7,9-dimethyl-1-phenyl-2,3,4,5-tetrahydro-1H-pyrrolo[1,2-a][1,4]diazepine

There total 6 articles about 7,9-dimethyl-1-phenyl-2,3,4,5-tetrahydro-1H-pyrrolo[1,2-a][1,4]diazepine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.8%

: 1030615-61-2
(Z)-7,9-dimethyl-1-phenyl-4,5-dihydro-3H-pyrrolo[1,2-a][1,4]diazepine

: 1030615-63-4
7,9-dimethyl-1-phenyl-2,3,4,5-tetrahydro-1H-pyrrolo[1,2-a][1,4]diazepine

Guidance literature:: With sodium tetrahydroborate; In methanol; at 0 ℃;

Reference yield:

: 93189-11-8
(3,5-dimethyl-1H-pyrrol-2-yl)(phenyl)methanone

: 1030615-63-4
7,9-dimethyl-1-phenyl-2,3,4,5-tetrahydro-1H-pyrrolo[1,2-a][1,4]diazepine

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 90 °C

2.1: hydrogenchloride / ethyl acetate / 4 h / 20 °C

2.2: pH 8 - 9

3.1: ethanol / Heating / reflux

4.1: sodium tetrahydroborate / methanol / 0 °C

With hydrogenchloride; sodium tetrahydroborate; potassium carbonate; In methanol; ethanol; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 625-82-1
2,4-dimethyl-1H-pyrrole

: 1030615-63-4
7,9-dimethyl-1-phenyl-2,3,4,5-tetrahydro-1H-pyrrolo[1,2-a][1,4]diazepine

Guidance literature:: Multi-step reaction with 5 steps

1.1: ethylmagnesium bromide / diethyl ether / 0.5 h / Heating / reflux

1.2: 20 °C

2.1: potassium carbonate / N,N-dimethyl-formamide / 90 °C

3.1: hydrogenchloride / ethyl acetate / 4 h / 20 °C

3.2: pH 8 - 9

4.1: ethanol / Heating / reflux

5.1: sodium tetrahydroborate / methanol / 0 °C

With hydrogenchloride; sodium tetrahydroborate; ethylmagnesium bromide; potassium carbonate; In methanol; diethyl ether; ethanol; ethyl acetate; N,N-dimethyl-formamide;