C₄₆H₅₂N₄O₁₀

Base Information

Chemical Name:C₄₆H₅₂N₄O₁₀
CAS No.:1268463-73-5
Molecular Formula:C₄₆H₅₂N₄O₁₀
Molecular Weight:820.94
Hs Code.:

C<sub>46</sub>H<sub>52</sub>N<sub>4</sub>O<sub>10</sub>

Synonyms:C₄₆H₅₂N₄O₁₀

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Chemical Property of C₄₆H₅₂N₄O₁₀

Chemical Property:

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Technology Process of C₄₆H₅₂N₄O₁₀

There total 12 articles about C₄₆H₅₂N₄O₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1268463-71-3
C₅₂H₆₆N₄O₁₀Si

: 1268463-73-5
C₄₆H₅₂N₄O₁₀

Guidance literature:: C₅₂H₆₆N₄O₁₀Si; With hydrogenchloride; In 1,4-dioxane; acetonitrile; at 20 ℃;

With hydrogen fluoride; water; In acetonitrile; at 20 ℃; for 16h;

With dipotassium hydrogenphosphate; In water; acetonitrile;

Reference yield:

: 2785-98-0
2,5-dimethoxybenzoic acid

: 1268463-73-5
C₄₆H₅₂N₄O₁₀

Guidance literature:: Multi-step reaction with 12 steps

1.1: 2,2,6,6-tetramethyl-piperidine; n-butyllithium / tetrahydrofuran / 2.5 h / 0 °C

1.2: 2 h / 25 °C

2.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 1 h / 25 °C

3.1: dmap; triethylamine / dichloromethane / 12 h / 25 °C

4.1: boron tribromide / dichloromethane / 1.5 h / -78 - 25 °C

5.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 20 °C

5.2: 20 °C

6.1: acetic anhydride; copper(II) nitrate hydrate / 3 h / 0 - 20 °C

7.1: sodium dithionite / water; tetrahydrofuran / 20 °C

8.1: dmap / N,N-dimethyl-formamide / 5 h / 20 °C

9.1: N,N,N,N,-tetramethylethylenediamine; diisopropylamine; n-butyllithium / tetrahydrofuran; hexanes / 0.5 h / -78 °C

9.2: 2 h / -100 - -20 °C

10.1: hydrogenchloride / 1,4-dioxane / 20 °C

11.1: acetic acid; sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 1 h / 20 °C

11.2: pH 7 / Phosphate buffer

12.1: hydrogenchloride / 1,4-dioxane; acetonitrile / 20 °C

12.2: 16 h / 20 °C

With 2,2,6,6-tetramethyl-piperidine; hydrogenchloride; dmap; n-butyllithium; sodium dithionite; oxalyl dichloride; copper(II) nitrate hydrate; N,N,N,N,-tetramethylethylenediamine; acetic anhydride; boron tribromide; sodium tris(acetoxy)borohydride; sodium hydride; acetic acid; triethylamine; diisopropylamine; N,N-dimethyl-formamide; In tetrahydrofuran; 1,4-dioxane; hexanes; dichloromethane; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 116324-66-4
2,5-Dimethoxy-6-methylbenzoesaeure

: 1268463-73-5
C₄₆H₅₂N₄O₁₀

Guidance literature:: Multi-step reaction with 11 steps

1.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 1 h / 25 °C

2.1: dmap; triethylamine / dichloromethane / 12 h / 25 °C

3.1: boron tribromide / dichloromethane / 1.5 h / -78 - 25 °C

4.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 20 °C

4.2: 20 °C

5.1: acetic anhydride; copper(II) nitrate hydrate / 3 h / 0 - 20 °C

6.1: sodium dithionite / water; tetrahydrofuran / 20 °C

7.1: dmap / N,N-dimethyl-formamide / 5 h / 20 °C

8.1: N,N,N,N,-tetramethylethylenediamine; diisopropylamine; n-butyllithium / tetrahydrofuran; hexanes / 0.5 h / -78 °C

8.2: 2 h / -100 - -20 °C

9.1: hydrogenchloride / 1,4-dioxane / 20 °C

10.1: acetic acid; sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 1 h / 20 °C

10.2: pH 7 / Phosphate buffer

11.1: hydrogenchloride / 1,4-dioxane; acetonitrile / 20 °C

11.2: 16 h / 20 °C

With hydrogenchloride; dmap; n-butyllithium; sodium dithionite; oxalyl dichloride; copper(II) nitrate hydrate; N,N,N,N,-tetramethylethylenediamine; acetic anhydride; boron tribromide; sodium tris(acetoxy)borohydride; sodium hydride; acetic acid; triethylamine; diisopropylamine; N,N-dimethyl-formamide; In tetrahydrofuran; 1,4-dioxane; hexanes; dichloromethane; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetonitrile;