3,4,5-tri-O-benzyl-1,2-O-cyclohexylidene-6-O-para-methoxybenzyl-D(L)-myo-inositol

Base Information

Chemical Name:3,4,5-tri-O-benzyl-1,2-O-cyclohexylidene-6-O-para-methoxybenzyl-D(L)-myo-inositol
CAS No.:132360-45-3
Molecular Formula:C₄₁H₄₆O₇
Molecular Weight:650.812
Hs Code.:

Synonyms:3,4,5-tri-O-benzyl-1,2-O-cyclohexylidene-6-O-para-methoxybenzyl-D(L)-myo-inositol

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Chemical Property of 3,4,5-tri-O-benzyl-1,2-O-cyclohexylidene-6-O-para-methoxybenzyl-D(L)-myo-inositol

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Technology Process of 3,4,5-tri-O-benzyl-1,2-O-cyclohexylidene-6-O-para-methoxybenzyl-D(L)-myo-inositol

There total 5 articles about 3,4,5-tri-O-benzyl-1,2-O-cyclohexylidene-6-O-para-methoxybenzyl-D(L)-myo-inositol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 100-39-0
benzyl bromide

: 132360-44-2
3-O-benzyl-1,2-O-cyclohexylidene-6-O-para-methoxybenzyl-D(L)-myo-inositol

: 132360-45-3
3,4,5-tri-O-benzyl-1,2-O-cyclohexylidene-6-O-para-methoxybenzyl-D(L)-myo-inositol

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 16h;
DOI:10.1016/S0040-4020(01)81480-0

Reference yield:

: 100-39-0
benzyl bromide

: 132360-45-3
3,4,5-tri-O-benzyl-1,2-O-cyclohexylidene-6-O-para-methoxybenzyl-D(L)-myo-inositol

Guidance literature:: Multi-step reaction with 4 steps

1: 70 percent / barium oxide/ barium hydroxide octahydrate / dimethylformamide / 96 h / Ambient temperature

2: 64.3 percent / NaH / dimethylformamide / 6 h / 20 °C

3: 57.3 percent / p-toluenesulfonic acid monohydrate, ethylene glycol / CH₂Cl₂

4: 85 percent / NaH / dimethylformamide / 16 h / 20 °C

With barium hydroxide octahydrate; sodium hydride; toluene-4-sulfonic acid; ethylene glycol; barium(II) oxide; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)81480-0

Reference yield:

: 23393-20-6,111901-82-7,120202-94-0,126722-28-9,134109-10-7,134109-11-8,136375-66-1
(+/-)-3-O-benzyl-1,2:4,5-di-O,O-cyclohexylidene-myo-inositol

: 132360-45-3
3,4,5-tri-O-benzyl-1,2-O-cyclohexylidene-6-O-para-methoxybenzyl-D(L)-myo-inositol

Guidance literature:: Multi-step reaction with 3 steps

1: 64.3 percent / NaH / dimethylformamide / 6 h / 20 °C

2: 57.3 percent / p-toluenesulfonic acid monohydrate, ethylene glycol / CH₂Cl₂

3: 85 percent / NaH / dimethylformamide / 16 h / 20 °C

With sodium hydride; toluene-4-sulfonic acid; ethylene glycol; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)81480-0