methyl 2,2-diphenylbutyrate

Base Information

• Chemical Name: methyl 2,2-diphenylbutyrate
• CAS No.: 79328-68-0
• Molecular Formula: C₁₇H₁₈O₂
• Molecular Weight: 254.329
• Mol file: 79328-68-0.mol

Synonyms:methyl 2,2-diphenylbutyrate

Chemical Property of methyl 2,2-diphenylbutyrate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of methyl 2,2-diphenylbutyrate

There total 5 articles about methyl 2,2-diphenylbutyrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.8%

methyl 4-(ethylthio)-2,2-diphenylbutyrate (79313-57-8) → methyl 2,2-diphenylbutyrate (79328-68-0)

Guidance literature:

nickel; In ethanol; for 15h; Heating;

DOI:10.1021/jo00338a020

Reference yield:

3,3-Diphenyl-dihydro-furan-2-one (956-89-8) → methyl 2,2-diphenylbutyrate (79328-68-0)

Guidance literature:

Multi-step reaction with 3 steps

1: 88 percent / AlBr₃ / 43.3 h / Ambient temperature

2: 98 percent / diethyl ether

3: 88.8 percent / Raney Ni / aq. ethanol / 15 h / Heating

With aluminum tri-bromide; nickel; In diethyl ether; ethanol;

DOI:10.1021/jo00338a020

Reference yield:

4-(ethylthio)-2,2-diphenylbutyric acid (71057-16-4) → methyl 2,2-diphenylbutyrate (79328-68-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 98 percent / diethyl ether

2: 88.8 percent / Raney Ni / aq. ethanol / 15 h / Heating

nickel; In diethyl ether; ethanol;

DOI:10.1021/jo00338a020

upstream raw materials:

methyl 4-(ethylthio)-2,2-diphenylbutyrate

ethyl bromide

3,3-Diphenyl-dihydro-furan-2-one

4-(ethylthio)-2,2-diphenylbutyric acid

Downstream raw materials:

2,2-diphenyl-butyric acid-(3-dimethylamino-1-methyl-propyl ester)

2,2-diphenyl-butyric acid-(3-dimethylamino-propyl ester)

2,2-diphenyl-butyryl chloride

2,2-diphenylbutanoic acid

Refernces