N-[1-{2-[2-(tert-Butyl-diphenyl-silanyloxy)-ethyl]-4,5-dimethoxy-phenyl}-2-(3,4-dimethoxy-phenyl)-ethyl]-acetamide

Base Information

Chemical Name:N-[1-{2-[2-(tert-Butyl-diphenyl-silanyloxy)-ethyl]-4,5-dimethoxy-phenyl}-2-(3,4-dimethoxy-phenyl)-ethyl]-acetamide
CAS No.:177726-02-2
Molecular Formula:C₃₈H₄₇NO₆Si
Molecular Weight:641.88
Hs Code.:

Synonyms:N-[1-{2-[2-(tert-Butyl-diphenyl-silanyloxy)-ethyl]-4,5-dimethoxy-phenyl}-2-(3,4-dimethoxy-phenyl)-ethyl]-acetamide

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Chemical Property of N-[1-{2-[2-(tert-Butyl-diphenyl-silanyloxy)-ethyl]-4,5-dimethoxy-phenyl}-2-(3,4-dimethoxy-phenyl)-ethyl]-acetamide

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Technology Process of N-[1-{2-[2-(tert-Butyl-diphenyl-silanyloxy)-ethyl]-4,5-dimethoxy-phenyl}-2-(3,4-dimethoxy-phenyl)-ethyl]-acetamide

There total 3 articles about N-[1-{2-[2-(tert-Butyl-diphenyl-silanyloxy)-ethyl]-4,5-dimethoxy-phenyl}-2-(3,4-dimethoxy-phenyl)-ethyl]-acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 75-36-5
acetyl chloride

: 173030-97-2
1-<2-<2-<(tert-butyldiphenylsilyl)oxy>ethyl>-4,5-dimethoxyphenyl>-2-(3,4-dimethoxyphenyl)ethylamine

: 177726-02-2
N-[1-{2-[2-(tert-Butyl-diphenyl-silanyloxy)-ethyl]-4,5-dimethoxy-phenyl}-2-(3,4-dimethoxy-phenyl)-ethyl]-acetamide

Guidance literature:: With dmap; triethylamine; In dichloromethane; for 4h; Ambient temperature;
DOI:10.1021/jo960007s

Reference yield:

: 1-{2-[2-(tert-Butyl-diphenyl-silanyloxy)-ethyl]-4,5-dimethoxy-phenyl}-2-(3,4-dimethoxy-phenyl)-ethanone oxime

: 177726-02-2
N-[1-{2-[2-(tert-Butyl-diphenyl-silanyloxy)-ethyl]-4,5-dimethoxy-phenyl}-2-(3,4-dimethoxy-phenyl)-ethyl]-acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: 60 percent / NaBH₄, TiCl₄ / 1,2-dimethoxy-ethane / 14 h / Ambient temperature

2: 85 percent / Et₃N, DMAP / CH₂Cl₂ / 4 h / Ambient temperature

With dmap; sodium tetrahydroborate; titanium tetrachloride; triethylamine; In 1,2-dimethoxyethane; dichloromethane;
DOI:10.1021/jo960007s

Reference yield:

: 108-24-7
acetic anhydride

: 1-{2-[2-(tert-Butyl-diphenyl-silanyloxy)-ethyl]-4,5-dimethoxy-phenyl}-2-(3,4-dimethoxy-phenyl)-ethanone oxime

: 177726-02-2
N-[1-{2-[2-(tert-Butyl-diphenyl-silanyloxy)-ethyl]-4,5-dimethoxy-phenyl}-2-(3,4-dimethoxy-phenyl)-ethyl]-acetamide

Guidance literature:: With tributylphosphine; sodium cyanoborohydride; acetic acid; diphenyldisulfane; Yield given. Multistep reaction;
DOI:10.1021/jo960007s