Technology Process of C20H28O6S
There total 7 articles about C20H28O6S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
methanol; sodium methylate;
at 20 ℃;
for 18h;
DOI:10.1039/c3ob42277a
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: toluene-4-sulfonic acid / acetone / 3 h / 20 °C / Enzymatic reaction
2.1: sodium hydride / N,N-dimethyl-formamide / 18 h / 0 - 20 °C / Inert atmosphere
3.1: acetic acid / water / 18 h / 50 °C
4.1: camphor-10-sulfonic acid / acetonitrile / 20 °C / Inert atmosphere
4.2: 0.25 h / 20 °C / Inert atmosphere
5.1: dicyclohexyl-carbodiimide; triethylamine; dmap / dichloromethane / 18 h / 20 °C
6.1: sodium methylate; methanol / 18 h / 20 °C
With
methanol; dmap; camphor-10-sulfonic acid; sodium methylate; sodium hydride; toluene-4-sulfonic acid; acetic acid; triethylamine; dicyclohexyl-carbodiimide;
In
dichloromethane; water; N,N-dimethyl-formamide; acetone; acetonitrile;
DOI:10.1039/c3ob42277a
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: sodium hydride / N,N-dimethyl-formamide / 18 h / 0 - 20 °C / Inert atmosphere
2.1: acetic acid / water / 18 h / 50 °C
3.1: camphor-10-sulfonic acid / acetonitrile / 20 °C / Inert atmosphere
3.2: 0.25 h / 20 °C / Inert atmosphere
4.1: dicyclohexyl-carbodiimide; triethylamine; dmap / dichloromethane / 18 h / 20 °C
5.1: sodium methylate; methanol / 18 h / 20 °C
With
methanol; dmap; camphor-10-sulfonic acid; sodium methylate; sodium hydride; acetic acid; triethylamine; dicyclohexyl-carbodiimide;
In
dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1039/c3ob42277a
