3,4-methylenedioxy-5,4'-dimethoxy-3'-[O,N^α-di(bis-benzylphosphoryl)-L-Tyr]-amido-Z-stilbene

Base Information

• Chemical Name: 3,4-methylenedioxy-5,4'-dimethoxy-3'-[O,N^α-di(bis-benzylphosphoryl)-L-Tyr]-amido-Z-stilbene
• CAS No.: 865717-74-4
• Molecular Formula: C₅₄H₅₂N₂O₁₂P₂
• Molecular Weight: 982.961

Synonyms:3,4-methylenedioxy-5,4'-dimethoxy-3'-[O,N^α-di(bis-benzylphosphoryl)-L-Tyr]-amido-Z-stilbene

Chemical Property of 3,4-methylenedioxy-5,4'-dimethoxy-3'-[O,N^α-di(bis-benzylphosphoryl)-L-Tyr]-amido-Z-stilbene

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Technology Process of 3,4-methylenedioxy-5,4'-dimethoxy-3'-[O,N^α-di(bis-benzylphosphoryl)-L-Tyr]-amido-Z-stilbene

There total 2 articles about 3,4-methylenedioxy-5,4'-dimethoxy-3'-[O,N^α-di(bis-benzylphosphoryl)-L-Tyr]-amido-Z-stilbene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

dibenzyl hydrogen phosphite (538-60-3) + 3,4-methylenedioxy-5,4'-dimethoxy-3'-(Nα-L-Tyr)-amido-Z-stilbene (501034-05-5) → 3,4-methylenedioxy-5,4'-dimethoxy-3'-[O,Nα-di(bis-benzylphosphoryl)-L-Tyr]-amido-Z-stilbene (865717-74-4)

Guidance literature:

With tetrachloromethane; dmap; N-ethyl-N,N-diisopropylamine; In acetonitrile; at -10 ℃; for 1h;

DOI:10.1021/np058033l

Reference yield:

Dibenzyl phosphite (17176-77-1) → 3,4-methylenedioxy-5,4'-dimethoxy-3'-[O,Nα-di(bis-benzylphosphoryl)-L-Tyr]-amido-Z-stilbene (865717-74-4)

Guidance literature:

C₂₆H₂₅ClN₂O₅; With dmap; N-ethyl-N,N-diisopropylamine; In acetonitrile; at -10 ℃; for 0.0166667h;

Dibenzyl phosphite; In acetonitrile; at -10 ℃; for 1h;

With potassium dihydrogenphosphate; In water; acetonitrile; at 20 ℃;

Reference yield:

3,4-methylenedioxy-5,4'-dimethoxy-3'-[O,Nα-di(bis-benzylphosphoryl)-L-Tyr]-amido-Z-stilbene (865717-74-4) → C26H28N2O12P2

Guidance literature:

With trimethylsilyl bromide; In dichloromethane; at 0 ℃; for 0.5h;

DOI:10.1021/np058033l

upstream raw materials:

Dibenzyl phosphite

dibenzyl hydrogen phosphite

3,4-methylenedioxy-5,4'-dimethoxy-3'-(N^α-L-Tyr)-amido-Z-stilbene

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