2,3-bis-2Z-butene-1,4-dinitrile

Base Information

Chemical Name:2,3-bis-2Z-butene-1,4-dinitrile
CAS No.:158985-44-5
Molecular Formula:C₂₄H₂₄N₄
Molecular Weight:368.481
Hs Code.:

2,3-bis<allyl(benzyl)amino>-2Z-butene-1,4-dinitrile

Synonyms:2,3-bis-2Z-butene-1,4-dinitrile

Suppliers and Price of 2,3-bis-2Z-butene-1,4-dinitrile

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2,3-bis-2Z-butene-1,4-dinitrile

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2,3-bis-2Z-butene-1,4-dinitrile

There total 5 articles about 2,3-bis-2Z-butene-1,4-dinitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 51802-04-1
N,N'-dibenzyldiaminomaleonitrile

: 158985-44-5
2,3-bis-2Z-butene-1,4-dinitrile

Guidance literature:: With sodium hydride; In tetrahydrofuran;
DOI:10.1039/c39940002095

Reference yield:

: 946529-80-2
(2Z)-2-Amino-3-{[(1E)-(phenyl)methylidene]-amino}but-2-enedinitrile

: 158985-44-5
2,3-bis-2Z-butene-1,4-dinitrile

Guidance literature:: Multi-step reaction with 4 steps

1.1: NaBH₄ / methanol; tetrahydrofuran

2.1: methanol / Heating

3.1: NaBH₄ / methanol; tetrahydrofuran

4.1: NaH / tetrahydrofuran / 0.5 h / -22 °C

4.2: 80 percent / tetrahydrofuran / 4 h / -22 - 20 °C

With sodium tetrahydroborate; sodium hydride; In tetrahydrofuran; methanol;
DOI:10.1016/j.tet.2005.03.090

Reference yield:

: (Z)-2-Benzylamino-3-{[1-phenyl-meth-(E)-ylidene]-amino}-but-2-enedinitrile

: 158985-44-5
2,3-bis-2Z-butene-1,4-dinitrile

Guidance literature:: Multi-step reaction with 2 steps

1.1: NaBH₄ / methanol; tetrahydrofuran

2.1: NaH / tetrahydrofuran / 0.5 h / -22 °C

2.2: 80 percent / tetrahydrofuran / 4 h / -22 - 20 °C

With sodium tetrahydroborate; sodium hydride; In tetrahydrofuran; methanol;
DOI:10.1016/j.tet.2005.03.090