2,3,4-Furantricarboxylic acid, 5-(dimethylamino)-, trimethyl ester (9CI)

Base Information

• Chemical Name: 2,3,4-Furantricarboxylic acid, 5-(dimethylamino)-, trimethyl ester (9CI)
• CAS No.: 191085-54-8
• Molecular Formula: C₁₂H₁₅NO₇
• Molecular Weight: 285.254
• Mol file: 191085-54-8.mol

Synonyms:2,3,4-Furantricarboxylicacid, 5-(dimethylamino)-, trimethyl ester (9CI)

Chemical Property of 2,3,4-Furantricarboxylic acid, 5-(dimethylamino)-, trimethyl ester (9CI)

Chemical Property:

• PSA: 0.00000
• LogP: 0.00000

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

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Technology Process of 2,3,4-Furantricarboxylic acid, 5-(dimethylamino)-, trimethyl ester (9CI)

There total 4 articles about 2,3,4-Furantricarboxylic acid, 5-(dimethylamino)-, trimethyl ester (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 28.0%

dimethyl acetylenedicarboxylate (762-42-5) + N'-(2-diazo-2-methyloxycarbonylacetyl)-N,N,N'-trimethylurea (191085-49-1) → trimethyl 5-dimethylamino-2,3,4-furan tricarboxylate (191085-54-8) + trimethyl 3-dimethylamino-1-methyl-2,6-dioxo-1,2,3,6-tetrahydro-3,4,5-pyridinetricarboxylate + C8H12N2O4

Guidance literature:

With rhodium(II) acetate; In toluene; for 0.333333h; Heating;

DOI:10.1021/ja001088j

Reference yield: 18.0%

dimethyl acetylenedicarboxylate (762-42-5) + N'-(2-diazo-2-methyloxycarbonylacetyl)-N,N,N'-trimethylurea (191085-49-1) → 1,1,3-trimethyl-5-methoxycarbonyl-2-oxo-2,3-dihydro-1H-imidazol-1-ium-4-olate (191085-50-4) + trimethyl 5-dimethylamino-2,3,4-furan tricarboxylate (191085-54-8) + trimethyl 3-dimethylamino-1-methyl-2,6-dioxo-1,2,3,6-tetrahydro-3,4,5-pyridinetricarboxylate

Guidance literature:

dirhodium tetraacetate; In toluene; Heating;

DOI:10.1016/S0040-4039(97)00618-7

Reference yield: 15.0%

dimethyl acetylenedicarboxylate (762-42-5) + 1,1,3-trimethyl-5-methoxycarbonyl-2-oxo-2,3-dihydro-1H-imidazol-1-ium-4-olate (191085-50-4) → trimethyl 5-dimethylamino-2,3,4-furan tricarboxylate (191085-54-8) + trimethyl 3-dimethylamino-1-methyl-2,6-dioxo-1,2,3,6-tetrahydro-3,4,5-pyridinetricarboxylate

Guidance literature:

dirhodium tetraacetate; In toluene; Heating;

DOI:10.1016/S0040-4039(97)00618-7

upstream raw materials:

dimethyl acetylenedicarboxylate

1,1,3-trimethyl-5-methoxycarbonyl-2-oxo-2,3-dihydro-1H-imidazol-1-ium-4-olate

N'-(2-diazo-2-methyloxycarbonylacetyl)-N,N,N'-trimethylurea

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