methyl 3,2',3'-tri-O-acetyl-4,4'-di-O-benzoyl-6,6'-dibromo-6,6'-dideoxy-β-sophoroside

Base Information

Chemical Name:methyl 3,2',3'-tri-O-acetyl-4,4'-di-O-benzoyl-6,6'-dibromo-6,6'-dideoxy-β-sophoroside
CAS No.:84730-69-8
Molecular Formula:C₃₃H₃₆Br₂O₁₄
Molecular Weight:816.448
Hs Code.:

Synonyms:methyl 3,2',3'-tri-O-acetyl-4,4'-di-O-benzoyl-6,6'-dibromo-6,6'-dideoxy-β-sophoroside

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Chemical Property of methyl 3,2',3'-tri-O-acetyl-4,4'-di-O-benzoyl-6,6'-dibromo-6,6'-dideoxy-β-sophoroside

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Technology Process of methyl 3,2',3'-tri-O-acetyl-4,4'-di-O-benzoyl-6,6'-dibromo-6,6'-dideoxy-β-sophoroside

There total 4 articles about methyl 3,2',3'-tri-O-acetyl-4,4'-di-O-benzoyl-6,6'-dibromo-6,6'-dideoxy-β-sophoroside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 84730-68-7
methyl 3,2',3'-tri-O-acetyl-4,6:4',6'-di-O-benzylidene-β-sophoroside

: 84730-69-8
methyl 3,2',3'-tri-O-acetyl-4,4'-di-O-benzoyl-6,6'-dibromo-6,6'-dideoxy-β-sophoroside

Guidance literature:: With N-Bromosuccinimide; barium carbonate; In tetrachloromethane; for 3h; Heating;
DOI:10.1016/0008-6215(83)88267-6

Reference yield:

: 16790-34-4
Methyl-2-O-(β-D-glucopyranosyl)-β-D-glcuopyranosid

: 84730-69-8
methyl 3,2',3'-tri-O-acetyl-4,4'-di-O-benzoyl-6,6'-dibromo-6,6'-dideoxy-β-sophoroside

Guidance literature:: Multi-step reaction with 3 steps

1: 82 percent / zinc chloride / 6 h / Ambient temperature

2: 92 percent / pyridine / Ambient temperature

3: 83 percent / barium carbonate, N-bromosuccinimide / CCl₄; various solvent(s) / 3 h / Heating

With N-Bromosuccinimide; barium carbonate; zinc(II) chloride; In pyridine; tetrachloromethane;
DOI:10.1016/0008-6215(83)88267-6

Reference yield:

: 100-52-7
benzaldehyde

: 84730-69-8
methyl 3,2',3'-tri-O-acetyl-4,4'-di-O-benzoyl-6,6'-dibromo-6,6'-dideoxy-β-sophoroside

Guidance literature:: Multi-step reaction with 3 steps

1: 82 percent / zinc chloride / 6 h / Ambient temperature

2: 92 percent / pyridine / Ambient temperature

3: 83 percent / barium carbonate, N-bromosuccinimide / CCl₄; various solvent(s) / 3 h / Heating

With N-Bromosuccinimide; barium carbonate; zinc(II) chloride; In pyridine; tetrachloromethane;
DOI:10.1016/0008-6215(83)88267-6