1-(3,5-bis-trifluoromethylphenyl)-2,2,2-trifluoro-1-(3-methyl-4-nitrophenyl)ethane

Base Information

Chemical Name:1-(3,5-bis-trifluoromethylphenyl)-2,2,2-trifluoro-1-(3-methyl-4-nitrophenyl)ethane
CAS No.:916975-32-1
Molecular Formula:C₁₇H₁₀F₉NO₂
Molecular Weight:431.258
Hs Code.:

Synonyms:1-(3,5-bis-trifluoromethylphenyl)-2,2,2-trifluoro-1-(3-methyl-4-nitrophenyl)ethane

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Chemical Property of 1-(3,5-bis-trifluoromethylphenyl)-2,2,2-trifluoro-1-(3-methyl-4-nitrophenyl)ethane

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Technology Process of 1-(3,5-bis-trifluoromethylphenyl)-2,2,2-trifluoro-1-(3-methyl-4-nitrophenyl)ethane

There total 6 articles about 1-(3,5-bis-trifluoromethylphenyl)-2,2,2-trifluoro-1-(3-methyl-4-nitrophenyl)ethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 916975-31-0
1-(3,5-bis-trifluoromethylphenyl)-2,2,2-trifluoro-1-(3-methyl-4-nitrophenyl)ethyl methanesulfonate

: 916975-32-1
1-(3,5-bis-trifluoromethylphenyl)-2,2,2-trifluoro-1-(3-methyl-4-nitrophenyl)ethane

Guidance literature:: 1-(3,5-bis-trifluoromethylphenyl)-2,2,2-trifluoro-1-(3-methyl-4-nitrophenyl)ethyl methanesulfonate; With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 ℃; for 0.5h;

With water; In tetrahydrofuran; diethyl ether;

Reference yield:

: 73852-19-4
3,5-bis-trifluromethylphenylboronic acid

: 916975-32-1
1-(3,5-bis-trifluoromethylphenyl)-2,2,2-trifluoro-1-(3-methyl-4-nitrophenyl)ethane

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,2-dimethoxyethane; water / 2 h / 85 °C

2.1: chromium(VI) oxide; acetic acid / 1 h / 20 °C

3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 8 h / 0 - 20 °C

3.3: 0.5 h / 20 °C

4.1: triethylamine / dichloromethane / 1 h / 0 - 20 °C

5.1: lithium aluminium tetrahydride / tetrahydrofuran / 0.5 h / 0 °C

With chromium(VI) oxide; lithium aluminium tetrahydride; tetrabutyl ammonium fluoride; sodium carbonate; acetic acid; triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; 1,2-dimethoxyethane; dichloromethane; water;

Reference yield:

: 18515-14-5
4-(chloromethyl)-2-methyl-1-nitro-benzene

: 916975-32-1
1-(3,5-bis-trifluoromethylphenyl)-2,2,2-trifluoro-1-(3-methyl-4-nitrophenyl)ethane

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,2-dimethoxyethane; water / 2 h / 85 °C

2.1: chromium(VI) oxide; acetic acid / 1 h / 20 °C

3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 8 h / 0 - 20 °C

3.3: 0.5 h / 20 °C

4.1: triethylamine / dichloromethane / 1 h / 0 - 20 °C

5.1: lithium aluminium tetrahydride / tetrahydrofuran / 0.5 h / 0 °C

With chromium(VI) oxide; lithium aluminium tetrahydride; tetrabutyl ammonium fluoride; sodium carbonate; acetic acid; triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; 1,2-dimethoxyethane; dichloromethane; water;