(5S,6S)-1,6,12-Tris-benzyloxy-9-chloro-5-hydroxy-8,11-dimethoxy-3-methyl-5,6-dihydro-benzo[a]anthracene-2-carboxylic acid methyl ester

Base Information

Chemical Name:(5S,6S)-1,6,12-Tris-benzyloxy-9-chloro-5-hydroxy-8,11-dimethoxy-3-methyl-5,6-dihydro-benzo[a]anthracene-2-carboxylic acid methyl ester
CAS No.:863423-83-0
Molecular Formula:C₄₄H₃₉ClO₈
Molecular Weight:731.242
Hs Code.:

Synonyms:(5S,6S)-1,6,12-Tris-benzyloxy-9-chloro-5-hydroxy-8,11-dimethoxy-3-methyl-5,6-dihydro-benzo[a]anthracene-2-carboxylic acid methyl ester

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Chemical Property of (5S,6S)-1,6,12-Tris-benzyloxy-9-chloro-5-hydroxy-8,11-dimethoxy-3-methyl-5,6-dihydro-benzo[a]anthracene-2-carboxylic acid methyl ester

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Technology Process of (5S,6S)-1,6,12-Tris-benzyloxy-9-chloro-5-hydroxy-8,11-dimethoxy-3-methyl-5,6-dihydro-benzo[a]anthracene-2-carboxylic acid methyl ester

There total 16 articles about (5S,6S)-1,6,12-Tris-benzyloxy-9-chloro-5-hydroxy-8,11-dimethoxy-3-methyl-5,6-dihydro-benzo[a]anthracene-2-carboxylic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 2-benzyloxy-3-[1-benzyloxy-3-(bis-benzyloxy-methyl)-6-chloro-5,8-dimethoxy-naphthalen-2-yl]-4-formyl-6-methyl-benzoic acid methyl ester

: 863423-83-0
(5S,6S)-1,6,12-Tris-benzyloxy-9-chloro-5-hydroxy-8,11-dimethoxy-3-methyl-5,6-dihydro-benzo[a]anthracene-2-carboxylic acid methyl ester

Guidance literature:: With methanol; samarium diiodide; boron trifluoride diethyl etherate; In tetrahydrofuran; at -78 - 0 ℃; for 0.183333h;
DOI:10.1002/anie.200501210

Reference yield: 60.0%

: 2-benzyloxy-3-[1-benzyloxy-3-(bis-benzyloxy-methyl)-6-chloro-5,8-dimethoxy-naphthalen-2-yl]-4-formyl-6-methyl-benzoic acid methyl ester

: 863423-83-0
(5S,6S)-1,6,12-Tris-benzyloxy-9-chloro-5-hydroxy-8,11-dimethoxy-3-methyl-5,6-dihydro-benzo[a]anthracene-2-carboxylic acid methyl ester

: 1007852-18-7
C₃₇H₃₁ClO₈

Guidance literature:: With samarium diiodide; titanium tetrachloride; In tetrahydrofuran; water; at -78 - 0 ℃;
DOI:10.1002/chem.200700863

Reference yield: 41.0%

: 2-benzyloxy-3-[1-benzyloxy-3-(bis-benzyloxy-methyl)-6-chloro-5,8-dimethoxy-naphthalen-2-yl]-4-formyl-6-methyl-benzoic acid methyl ester

: 863423-83-0
(5S,6S)-1,6,12-Tris-benzyloxy-9-chloro-5-hydroxy-8,11-dimethoxy-3-methyl-5,6-dihydro-benzo[a]anthracene-2-carboxylic acid methyl ester

: 1007852-13-2
C₄₄H₃₉ClO₈

Guidance literature:: With samarium diiodide; trimethylsilyl trifluoromethanesulfonate; In tetrahydrofuran; water; at -78 - 0 ℃;
DOI:10.1002/chem.200700863