N-((4,5-dimethoxy-9,10-dioxo-9,10-dihydroanthracen-2-yl)methyl)-N,N-dimethylbenzenaminium chloride

Base Information

Chemical Name:N-((4,5-dimethoxy-9,10-dioxo-9,10-dihydroanthracen-2-yl)methyl)-N,N-dimethylbenzenaminium chloride
CAS No.:1425441-27-5
Molecular Formula:C₂₅H₂₄NO₄*Cl
Molecular Weight:437.923
Hs Code.:

Synonyms:N-((4,5-dimethoxy-9,10-dioxo-9,10-dihydroanthracen-2-yl)methyl)-N,N-dimethylbenzenaminium chloride

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Chemical Property of N-((4,5-dimethoxy-9,10-dioxo-9,10-dihydroanthracen-2-yl)methyl)-N,N-dimethylbenzenaminium chloride

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Technology Process of N-((4,5-dimethoxy-9,10-dioxo-9,10-dihydroanthracen-2-yl)methyl)-N,N-dimethylbenzenaminium chloride

There total 3 articles about N-((4,5-dimethoxy-9,10-dioxo-9,10-dihydroanthracen-2-yl)methyl)-N,N-dimethylbenzenaminium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1425441-15-1
3-(chloromethyl)-1,8-dimethoxyanthracene-9,10-dione

: 121-69-7,77733-26-7
N,N-dimethyl-aniline

: 1425441-27-5
N-((4,5-dimethoxy-9,10-dioxo-9,10-dihydroanthracen-2-yl)methyl)-N,N-dimethylbenzenaminium chloride

Guidance literature:: In chloroform; at 20 ℃; for 336h;
DOI:10.1016/j.bmc.2013.01.015

Reference yield:

: 481-72-1
1,8-dihydroxy-3-hydroxymethyl-9,10-anthracenedione

: 1425441-27-5
N-((4,5-dimethoxy-9,10-dioxo-9,10-dihydroanthracen-2-yl)methyl)-N,N-dimethylbenzenaminium chloride

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / acetone / 12 h / 56 °C

2: thionyl chloride; N,N-dimethyl-formamide / 26 h / 20 °C

3: chloroform / 336 h / 20 °C

With thionyl chloride; potassium carbonate; N,N-dimethyl-formamide; In chloroform; acetone;
DOI:10.1016/j.bmc.2013.01.015

Reference yield:

: 50488-95-4
3-(hydroxymethyl)-1,8-dimethoxy-9,10-anthracenedione

: 1425441-27-5
N-((4,5-dimethoxy-9,10-dioxo-9,10-dihydroanthracen-2-yl)methyl)-N,N-dimethylbenzenaminium chloride

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride; N,N-dimethyl-formamide / 26 h / 20 °C

2: chloroform / 336 h / 20 °C

With thionyl chloride; N,N-dimethyl-formamide; In chloroform;
DOI:10.1016/j.bmc.2013.01.015