N-<2-(2-bromo-4,5-dimethoxyphenyl)-1-(3,4-dimethoxyphenyl)ethyl>formamide

Base Information

• Chemical Name: N-<2-(2-bromo-4,5-dimethoxyphenyl)-1-(3,4-dimethoxyphenyl)ethyl>formamide
• CAS No.: 90402-70-3
• Molecular Formula: C₁₉H₂₂BrNO₅
• Molecular Weight: 424.291

Synonyms:N-<2-(2-bromo-4,5-dimethoxyphenyl)-1-(3,4-dimethoxyphenyl)ethyl>formamide

Chemical Property of N-<2-(2-bromo-4,5-dimethoxyphenyl)-1-(3,4-dimethoxyphenyl)ethyl>formamide

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Technology Process of N-<2-(2-bromo-4,5-dimethoxyphenyl)-1-(3,4-dimethoxyphenyl)ethyl>formamide

There total 3 articles about N-<2-(2-bromo-4,5-dimethoxyphenyl)-1-(3,4-dimethoxyphenyl)ethyl>formamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

2-(2-Bromo-4,5-dimethoxy-phenyl)-1-(3,4-dimethoxy-phenyl)-ethanone → N-<2-(2-bromo-4,5-dimethoxyphenyl)-1-(3,4-dimethoxyphenyl)ethyl>formamide (90402-70-3) + (E)-1-(2-bromo-4,5-dimethoxyphenyl)-2-(3,4-dimethoxyphenyl)ethylene (84573-13-7) + 5-(2-bromo-4,5-dimethoxyphenyl)-4-(3,4-dimethoxyphenyl)pyrimidine

Guidance literature:

With formic acid; ammonium formate; formamide; at 185 - 190 ℃;

Reference yield: 4.0%

formamide (77287-34-4,77287-35-5,60100-09-6) + 2-(2-Bromo-4,5-dimethoxy-phenyl)-1-(3,4-dimethoxy-phenyl)-ethanone → N-<2-(2-bromo-4,5-dimethoxyphenyl)-1-(3,4-dimethoxyphenyl)ethyl>formamide (90402-70-3) + (E)-1-(2-bromo-4,5-dimethoxyphenyl)-2-(3,4-dimethoxyphenyl)ethylene (84573-13-7) + 5-(2-bromo-4,5-dimethoxyphenyl)-4-(3,4-dimethoxyphenyl)pyrimidine

Guidance literature:

With formic acid; ammonium formate; at 185 - 190 ℃;

Reference yield:

N-<1,2-bis(3,4-dimethoxyphenyl)ethyl>formamide (76306-70-2) → N-<2-(2-bromo-4,5-dimethoxyphenyl)-1-(3,4-dimethoxyphenyl)ethyl>formamide (90402-70-3) + (E)-1-(2-bromo-4,5-dimethoxyphenyl)-2-(3,4-dimethoxyphenyl)ethylene (84573-13-7)

Guidance literature:

With bromine; In acetic acid; for 2h; Ambient temperature; with 1 equivalent of Br₂;

upstream raw materials:

N-<1,2-bis(3,4-dimethoxyphenyl)ethyl>formamide

formamide

Downstream raw materials:

N-<2-(2-bromo-4,5-dimethoxyphenyl)-1-(3,4-dimethoxyphenyl)ethyl>benzamide

N-<2-(2-bromo-4,5-dimethoxyphenyl)-1-(3,4-dimethoxyphenyl)ethyl>acetamide

2-(2-bromo-4,5-dimethoxyphenyl)-1-(3,4-dimethoxyphenyl)ethylamine

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