76306-70-2

Upstream product

• 4927-55-3 1,2-bis(3,4-dimethoxyphenyl)ethanone 
• 540-69-2 ammonium formate 
• 77287-34-4 formamide 

Downstream Products

• 5471-40-9 3,4,3',4'-tetramethoxy-bibenzyl-α-ylamine 
• 69504-70-7 3-(3,4-dimethoxyphenyl)-6,7-dimethoxyisoquinoline 
• 20232-47-7 3-(3,4-dimethoxyphenyl)-6,7-dimethoxy-3,4-dihydroisoquinoline 
• 18513-98-9 3,4,3',4'-Tetramethoxystilben 
• 76306-53-1 1-(3,4-Dimethoxy-benzyl)-2,3-bis-(3,4-dimethoxy-phenyl)-5,6-dimethoxy-indan 
• 87419-46-3 3-(3,4-Dimethoxy-phenyl)-6,7-dimethoxy-3,4-dihydro-isoquinoline; hydrochloride 
• 90402-70-3 N-<2-(2-bromo-4,5-dimethoxyphenyl)-1-(3,4-dimethoxyphenyl)ethyl>formamide 
• 84573-13-7 (E)-1-(2-bromo-4,5-dimethoxyphenyl)-2-(3,4-dimethoxyphenyl)ethylene 
• 76306-62-2 N-<1,2-bis(3,4-dimethoxyphenyl)ethyl>acetamide 
• 87419-45-2 N-<1,2-bis(3,4-dimethoxyphenyl)ethyl>phenylacetamide 
• 76306-43-9 3,4-dihydro-6,7-dimethoxy-3-(3,4-dimethoxyphenyl)-1-methylisoquinoline 
• 135365-11-6 5-(3,4-Dimethoxy-phenyl)-8,9-dimethoxy-6,10b-dihydro-5H-oxazolo[2,3-a]isoquinoline-2,3-dione 
• 135365-12-7 5-(3,4-Dimethoxy-phenyl)-8,9-dimethoxy-10b-methyl-6,10b-dihydro-5H-oxazolo[2,3-a]isoquinoline-2,3-dione 
• 91486-74-7 3-(3,4-dimethoxyphenyl)-6,7-dimethoxy-3,4-dihydroisoquinoline methiodide 

Relevant academic research and scientific papers

Towards the rehabilitation of the Leuckart reductive amination reaction using microwave technology

Leuckart reductive amination of carbonyl compounds was dramatically enhanced with respect to conventional heating by a specific microwave effect when the reaction was performed, under solvent-free conditions, in a monomode microwave reactor. Excellent iso

Application of the intramolecular ?-amidoalkylation reaction for the synthesis of 3- and 1,3-alkyl(aryl) 2-formyltetrahydroisoquinolines

3- and 1,3-alkyl(aryl) 2-formyltetrahydroisoquinolines 6 are obtained by the application of the intramolecular ?-amidoalkylation reaction from 1-alkyl(aryl)-2-arylethylformamides 2 and aldehydes in acidic medium.

A Modified Bischler-Napieralski Procedure for the Synthesis of 3-Aryl-3,4-dihydroisoquinolines

A modification of the Bischler-Napieralski reaction for the cyclization of (1,2-diphenylethyl)amides to the 3-aryl-3,4-dihydroisoquinolines is presented.Elimination of the amide group as the nitrile via the retro-Ritter reaction is avoided by its conversion to an N-acyliminium intermediate with oxalyl chloride-FeCl3.Removal of the oxalyl group in refluxing MeOH-sulfuric acid provides the 3,4-dihydroisoquinolines in moderate to high yields.The method is also highly effective with (2-phenylethyl)amides.

ON THE LEUKART REACTION OFDEOXYBENZOINS: ISOLATION AND CHARAKTERIZATION OF 2,3,4,5-TETRAARYLPYRIDINE DERIVATIVES

The Leukart reaction of deoxybenzoins has been examined.The deoxybenzoins (1b-c) possessing a phenolic substituent in the ortho position to the carbonyl group react with formamide to afford, besides the known stilbene, pyrimidine and isoflavone derivative