diethyl (3-((5-(2-chlorophenyl)-1H-1,2,4-triazol-3-yl)thio)propyl)phosphonate

Base Information

Chemical Name:diethyl (3-((5-(2-chlorophenyl)-1H-1,2,4-triazol-3-yl)thio)propyl)phosphonate
CAS No.:1620200-75-0
Molecular Formula:C₁₅H₂₁ClN₃O₃PS
Molecular Weight:389.843
Hs Code.:

Synonyms:diethyl (3-((5-(2-chlorophenyl)-1H-1,2,4-triazol-3-yl)thio)propyl)phosphonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of diethyl (3-((5-(2-chlorophenyl)-1H-1,2,4-triazol-3-yl)thio)propyl)phosphonate

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Technology Process of diethyl (3-((5-(2-chlorophenyl)-1H-1,2,4-triazol-3-yl)thio)propyl)phosphonate

There total 6 articles about diethyl (3-((5-(2-chlorophenyl)-1H-1,2,4-triazol-3-yl)thio)propyl)phosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1186-10-3
diethyl (3-bromopropyl)phosphonate

: 58755-00-3
5-(2-chlorophenyl)-1,2-dihydro-1,2,4-triazole-3-thione

: 1620200-75-0
diethyl (3-((5-(2-chlorophenyl)-1H-1,2,4-triazol-3-yl)thio)propyl)phosphonate

Guidance literature:: With iron(III) oxide; In water; at 80 ℃; for 1h; chemoselective reaction; Green chemistry;
DOI:10.1080/00397911.2014.918146

Reference yield: 84.0%

: 1186-10-3
diethyl 3-(bromopropyl)phosphonic acid

: 58755-00-3
5-(2-chlorophenyl)-1,2-dihydro-1,2,4-triazole-3-thione

: 1620200-75-0
diethyl (3-((5-(2-chlorophenyl)-1H-1,2,4-triazol-3-yl)thio)propyl)phosphonate

Guidance literature:: With glycerol-based sulfonic acid functionalized carbon catalyst; In water; for 1h; chemoselective reaction; Reflux; Green chemistry;
DOI:10.2174/1570180813666160125222334

Reference yield:

: 610-96-8
methyl chlorobenzoate

: 1620200-75-0
diethyl (3-((5-(2-chlorophenyl)-1H-1,2,4-triazol-3-yl)thio)propyl)phosphonate

Guidance literature:: Multi-step reaction with 4 steps

1: hydrazine hydrate / methanol / 8 h / Reflux

2: hydrogenchloride / water / 3 h / Reflux

3: sodium hydroxide / water / 2 h / Reflux

4: iron(III) oxide / water / 1 h / 80 °C / Green chemistry

With hydrogenchloride; iron(III) oxide; hydrazine hydrate; sodium hydroxide; In methanol; water;
DOI:10.1080/00397911.2014.918146