B₁₀H₁₀CC₇H₁₅CCH₂C₆H₄I

Base Information

Chemical Name:B₁₀H₁₀CC₇H₁₅CCH₂C₆H₄I
CAS No.:1227007-92-2
Molecular Formula:C₁₆H₃₁B₁₀I
Molecular Weight:458.437
Hs Code.:

B<sub>10</sub>H<sub>10</sub>CC<sub>7</sub>H<sub>15</sub>CCH<sub>2</sub>C<sub>6</sub>H<sub>4</sub>I

Synonyms:B₁₀H₁₀CC₇H₁₅CCH₂C₆H₄I

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Chemical Property of B₁₀H₁₀CC₇H₁₅CCH₂C₆H₄I

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Technology Process of B₁₀H₁₀CC₇H₁₅CCH₂C₆H₄I

There total 1 articles about B₁₀H₁₀CC₇H₁₅CCH₂C₆H₄I which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 126223-53-8
1-(n-heptyl)-1,2-dicarba-closo-dodecaborane

: 16004-15-2
1-bromomethyl-4-iodobenzene

: 1227007-92-2
B₁₀H₁₀CC₇H₁₅CCH₂C₆H₄I

Guidance literature:: With n-butyllithium; In dimethylformamide; hexane; (Ar) n-butyllithium in hexane was added at 0°C to a soln. of carborane-compound in DME, stirred at 0°C for 1 h, IC6H4CH2Br in DME was added, refluxed at 90°C for 24 h, cooled to room temp.; filtered over silica gel pad, the solvent was removed, silica gel columnchromy. with hexane; as an oily liquid;
DOI:10.1021/ja101845m

Reference yield: 96.0%

: 1227007-92-2
B₁₀H₁₀CC₇H₁₅CCH₂C₆H₄I

: 108-24-7
acetic anhydride

: 1227007-93-3
B₁₀H₁₀CC₇H₁₅CCH₂C₆H₄COCH₃

Guidance literature:: With ethyl(diisopropyl)amine; LiCl; tris(dibenzylideneacetone)dipalladium ⁽⁰⁾; In dimethylformamide; (Ar) acetic anhydride, Pd-complex, amine-compound and LiCl were added toa soln. of carborane-compound in DME, the mixt. was stirred at 100.degr ee.C for 20 h, cooled to room temp.; filtered thorugh a silica gel pad, quenched with water, extd. with diethyl ether, the organic layer was dried over MgSO4, evapd., silica gel chromy. with 30% ethyl acetate in hexane as eluent; as oil: elem. anal.;
DOI:10.1021/ja101845m