Dimethylamino-(2,2,3-trimethyl-6-methylene-cyclohexyl)-acetonitrile

Base Information

Chemical Name:Dimethylamino-(2,2,3-trimethyl-6-methylene-cyclohexyl)-acetonitrile
CAS No.:107249-67-2
Molecular Formula:C₁₄H₂₄N₂
Molecular Weight:220.358
Hs Code.:

Synonyms:Dimethylamino-(2,2,3-trimethyl-6-methylene-cyclohexyl)-acetonitrile

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Chemical Property of Dimethylamino-(2,2,3-trimethyl-6-methylene-cyclohexyl)-acetonitrile

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Technology Process of Dimethylamino-(2,2,3-trimethyl-6-methylene-cyclohexyl)-acetonitrile

There total 6 articles about Dimethylamino-(2,2,3-trimethyl-6-methylene-cyclohexyl)-acetonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 526-75-0
2,3-Dimethylphenol

: 107249-67-2
Dimethylamino-(2,2,3-trimethyl-6-methylene-cyclohexyl)-acetonitrile

Guidance literature:: Multi-step reaction with 6 steps

1: 93 percent / H₂ / Raney Ni / hexane / 3 h / 140 °C

2: 86 percent / CrO₃, water, H₂SO₄ / acetone / 3 h / 20 °C

3: 1) 63 percent NaH; 2) HCOOEt, 12 percent aq. HCl / 1) mineral oil, toluene, 2 h, 100 deg C; 2 h, 60 deg C; 2) toluene, mineral oil, 12 h, RT

4: 97 percent / H₃PO₄ / 12 h / Ambient temperature

6: 1) methanesulfonyl chloride, NEt₃; 2) Na₂CO₃ / 1) ether, 2 h, 10 deg C; 2) MeCN, 4 h, reflux

With chromium(VI) oxide; hydrogenchloride; phosphoric acid; sulfuric acid; water; hydrogen; sodium hydride; sodium carbonate; methanesulfonyl chloride; triethylamine; formic acid ethyl ester; nickel; In hexane; acetone;

Reference yield:

: 1502-24-5
2,3-dimethylcyclohexan-1-ol

: 107249-67-2
Dimethylamino-(2,2,3-trimethyl-6-methylene-cyclohexyl)-acetonitrile

Guidance literature:: Multi-step reaction with 5 steps

1: 86 percent / CrO₃, water, H₂SO₄ / acetone / 3 h / 20 °C

2: 1) 63 percent NaH; 2) HCOOEt, 12 percent aq. HCl / 1) mineral oil, toluene, 2 h, 100 deg C; 2 h, 60 deg C; 2) toluene, mineral oil, 12 h, RT

3: 97 percent / H₃PO₄ / 12 h / Ambient temperature

5: 1) methanesulfonyl chloride, NEt₃; 2) Na₂CO₃ / 1) ether, 2 h, 10 deg C; 2) MeCN, 4 h, reflux

With chromium(VI) oxide; hydrogenchloride; phosphoric acid; sulfuric acid; water; sodium hydride; sodium carbonate; methanesulfonyl chloride; triethylamine; formic acid ethyl ester; In acetone;

Reference yield:

: 13395-76-1
2,3-dimethylcyclohexanone

: 107249-67-2
Dimethylamino-(2,2,3-trimethyl-6-methylene-cyclohexyl)-acetonitrile

Guidance literature:: Multi-step reaction with 4 steps

1: 1) 63 percent NaH; 2) HCOOEt, 12 percent aq. HCl / 1) mineral oil, toluene, 2 h, 100 deg C; 2 h, 60 deg C; 2) toluene, mineral oil, 12 h, RT

2: 97 percent / H₃PO₄ / 12 h / Ambient temperature

4: 1) methanesulfonyl chloride, NEt₃; 2) Na₂CO₃ / 1) ether, 2 h, 10 deg C; 2) MeCN, 4 h, reflux

With hydrogenchloride; phosphoric acid; sodium hydride; sodium carbonate; methanesulfonyl chloride; triethylamine; formic acid ethyl ester;