Technology Process of C30H33Cl2N7O10S2
There total 6 articles about C30H33Cl2N7O10S2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C63H74Cl2N7O15S2(1+)*I(1-);
With
aluminum (III) chloride;
In
nitromethane; dichloromethane; methoxybenzene;
at -40 - 0 ℃;
for 1.16667h;
With
hydrogenchloride;
In
nitromethane; dichloromethane; water; methoxybenzene; isopropyl alcohol;
at 0 ℃;
- Guidance literature:
-
2,5-dichloro-3,4-bis((4-methoxybenzyl)oxy)-N-(2-(pyrrolidin-1-yl)ethyl)benzamide; C39H44IN5O10S2;
In
N,N-dimethyl-formamide;
at 20 ℃;
for 8h;
Inert atmosphere;
With
acetyl chloride; potassium iodide;
In
N,N-dimethyl-formamide;
at 0 ℃;
for 1h;
Inert atmosphere;
With
aluminum (III) chloride; methoxybenzene;
In
nitromethane; dichloromethane;
at -40 - 0 ℃;
for 1.33333h;
Inert atmosphere;
DOI:10.1016/j.ejmech.2018.06.014
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 1 h / 70 °C
2.1: sodium hydroxide; water / tetrahydrofuran; methanol / 1 h / 70 °C
3.1: triethylamine; methanesulfonyl chloride / N,N-dimethyl acetamide / 1.17 h / -15 °C
3.2: 1 h / -15 °C
4.1: N,N-dimethyl-formamide / 5 h / 20 °C
4.2: 2 h / -40 - 0 °C
5.1: aluminum (III) chloride / dichloromethane; nitromethane; methoxybenzene / 1.17 h / -40 - 0 °C
5.2: 0 °C
With
aluminum (III) chloride; water; potassium carbonate; methanesulfonyl chloride; triethylamine; potassium iodide; sodium hydroxide;
In
tetrahydrofuran; methanol; nitromethane; dichloromethane; N,N-dimethyl acetamide; methoxybenzene; N,N-dimethyl-formamide;
