2,5-dimethoxy-3-[2-(phenylmethoxy)ethyl]-4-[(phenylmethoxy)methyl]benzaldehyde

Base Information

Chemical Name:2,5-dimethoxy-3-[2-(phenylmethoxy)ethyl]-4-[(phenylmethoxy)methyl]benzaldehyde
CAS No.:327164-01-2
Molecular Formula:C₂₆H₂₈O₅
Molecular Weight:420.505
Hs Code.:

Synonyms:2,5-dimethoxy-3-[2-(phenylmethoxy)ethyl]-4-[(phenylmethoxy)methyl]benzaldehyde

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Chemical Property of 2,5-dimethoxy-3-[2-(phenylmethoxy)ethyl]-4-[(phenylmethoxy)methyl]benzaldehyde

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Technology Process of 2,5-dimethoxy-3-[2-(phenylmethoxy)ethyl]-4-[(phenylmethoxy)methyl]benzaldehyde

There total 6 articles about 2,5-dimethoxy-3-[2-(phenylmethoxy)ethyl]-4-[(phenylmethoxy)methyl]benzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 327164-07-8
1,4-dimethoxy-3-[2-(phenylmethoxy)ethyl]-2-[(phenylmethoxy)methyl]-5-(1-propenyl)benzene

: 327164-01-2
2,5-dimethoxy-3-[2-(phenylmethoxy)ethyl]-4-[(phenylmethoxy)methyl]benzaldehyde

Guidance literature:: 1,4-dimethoxy-3-[2-(phenylmethoxy)ethyl]-2-[(phenylmethoxy)methyl]-5-(1-propenyl)benzene; With ozone; sudan II; In dichloromethane; at -78 ℃;

With triphenylphosphine; In dichloromethane; for 2h; Further stages.; cooling;
DOI:10.1021/jo001523s

Reference yield:

: 100-39-0
benzyl bromide

: 327164-01-2
2,5-dimethoxy-3-[2-(phenylmethoxy)ethyl]-4-[(phenylmethoxy)methyl]benzaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1.1: 68 percent / NaH / tetrahydrofuran / 3 h / 0 °C

2.1: 89 percent / RhCl₃*3H₂O / toluene; methanol / 3 h / Heating

3.1: O₃; sudan II red / CH₂Cl₂ / -78 °C

3.2: 76 percent / Ph₃P / CH₂Cl₂ / 2 h / cooling

With rhodium(III) chloride; sodium hydride; ozone; sudan II; In tetrahydrofuran; methanol; dichloromethane; toluene;
DOI:10.1021/jo001523s

Reference yield:

: 327163-87-1
5,8-dimethoxy-6-(2-propenyl)isochroman-3-ol

: 327164-01-2
2,5-dimethoxy-3-[2-(phenylmethoxy)ethyl]-4-[(phenylmethoxy)methyl]benzaldehyde

Guidance literature:: Multi-step reaction with 4 steps

1.1: 90 percent / NaBH₄ / methanol / 1 h / 0 °C

2.1: 68 percent / NaH / tetrahydrofuran / 3 h / 0 °C

3.1: 89 percent / RhCl₃*3H₂O / toluene; methanol / 3 h / Heating

4.1: O₃; sudan II red / CH₂Cl₂ / -78 °C

4.2: 76 percent / Ph₃P / CH₂Cl₂ / 2 h / cooling

With sodium tetrahydroborate; rhodium(III) chloride; sodium hydride; ozone; sudan II; In tetrahydrofuran; methanol; dichloromethane; toluene;
DOI:10.1021/jo001523s