N,N-diethyl-2-(4-methylphenyl)-ethanamine

Base Information

Chemical Name:N,N-diethyl-2-(4-methylphenyl)-ethanamine
CAS No.:17734-31-5
Molecular Formula:C₁₃H₂₁N
Molecular Weight:191.316
Hs Code.:

Synonyms:N,N-diethyl-2-(4-methylphenyl)-ethanamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N-diethyl-2-(4-methylphenyl)-ethanamine

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Technology Process of N,N-diethyl-2-(4-methylphenyl)-ethanamine

There total 10 articles about N,N-diethyl-2-(4-methylphenyl)-ethanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₃H₁₉N

: 17734-31-5
N,N-diethyl-2-(4-methylphenyl)-ethanamine

Guidance literature:: With sodium tris(acetoxy)borohydride; acetic acid; In 1,2-dichloro-ethane; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1246/cl.130485

Reference yield:

: 766-97-2
4-n-methylphenylacetylene

: 17734-31-5
N,N-diethyl-2-(4-methylphenyl)-ethanamine

Guidance literature:: Multi-step reaction with 3 steps

1: Schwartz's reagent / toluene / 20 h / 20 °C / Inert atmosphere; Schlenk technique

2: triethyl phosphite; lithium tert-butoxide; copper(II) acetate monohydrate / tetrahydrofuran / 4 h / 20 °C / Inert atmosphere; Schlenk technique

3: sodium tris(acetoxy)borohydride; acetic acid / 1,2-dichloro-ethane / 1 h / 20 °C / Inert atmosphere

With Schwartz's reagent; copper(II) acetate monohydrate; sodium tris(acetoxy)borohydride; acetic acid; lithium tert-butoxide; triethyl phosphite; In tetrahydrofuran; 1,2-dichloro-ethane; toluene;
DOI:10.1246/cl.130485

Reference yield:

: 1377187-54-6
4,4,5,5-tetramethyl-2-(2-p-tolylvinyl)[1,3,2]dioxaborolane

: 17734-31-5
N,N-diethyl-2-(4-methylphenyl)-ethanamine

Guidance literature:: Multi-step reaction with 2 steps

1: triethyl phosphite; lithium tert-butoxide; copper(II) acetate monohydrate / tetrahydrofuran / 4 h / 20 °C / Inert atmosphere; Schlenk technique

2: sodium tris(acetoxy)borohydride; acetic acid / 1,2-dichloro-ethane / 1 h / 20 °C / Inert atmosphere

With copper(II) acetate monohydrate; sodium tris(acetoxy)borohydride; acetic acid; lithium tert-butoxide; triethyl phosphite; In tetrahydrofuran; 1,2-dichloro-ethane;
DOI:10.1246/cl.130485