2-(2-nitro-5-morpholinophenyl)-4-(4-chlorophenyl)-1,2-dihydro-1-phthalazinone

Base Information

• Chemical Name: 2-(2-nitro-5-morpholinophenyl)-4-(4-chlorophenyl)-1,2-dihydro-1-phthalazinone
• CAS No.: 591735-72-7
• Molecular Formula: C₂₄H₁₉ClN₄O₄
• Molecular Weight: 462.892

Synonyms:2-(2-nitro-5-morpholinophenyl)-4-(4-chlorophenyl)-1,2-dihydro-1-phthalazinone

Chemical Property of 2-(2-nitro-5-morpholinophenyl)-4-(4-chlorophenyl)-1,2-dihydro-1-phthalazinone

Chemical Property:

Purity/Quality:

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Technology Process of 2-(2-nitro-5-morpholinophenyl)-4-(4-chlorophenyl)-1,2-dihydro-1-phthalazinone

There total 2 articles about 2-(2-nitro-5-morpholinophenyl)-4-(4-chlorophenyl)-1,2-dihydro-1-phthalazinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-(4-chlorobenzoyl)benzoic acid (85-56-3) → 2-(2-nitro-5-morpholinophenyl)-4-(4-chlorophenyl)-1,2-dihydro-1-phthalazinone (591735-72-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 53 percent / sulfuric acid / ethanol / 1 h / 100 - 120 °C

2: 77 percent / 1.5 h / Heating

With sulfuric acid; In ethanol;

DOI:10.1016/j.tet.2006.07.089

Reference yield:

5-chloro-2-nitrophenylhydrazine (1966-16-1) → 2-(2-nitro-5-morpholinophenyl)-4-(4-chlorophenyl)-1,2-dihydro-1-phthalazinone (591735-72-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 53 percent / sulfuric acid / ethanol / 1 h / 100 - 120 °C

2: 77 percent / 1.5 h / Heating

With sulfuric acid; In ethanol;

DOI:10.1016/j.tet.2006.07.089

Reference yield: 85.0%

2-(2-nitro-5-morpholinophenyl)-4-(4-chlorophenyl)-1,2-dihydro-1-phthalazinone (591735-72-7) → 5-(4-chlorophenyl)-9-morpholino-benzo[4,5]imidazo[2,1-a]phthalazine

Guidance literature:

With phosphoric acid; iron; at 100 - 140 ℃;

DOI:10.1016/j.tet.2006.07.089

upstream raw materials:

2-(4-chlorobenzoyl)benzoic acid

5-chloro-2-nitrophenylhydrazine

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