2-(3-methoxy-1-(1-(3-(3-methoxyphenoxy)-4-methylpentyl)piperidin-4-yl)-2-oxoindolin-3-yl)-N-methylacetamide

Base Information

Chemical Name:2-(3-methoxy-1-(1-(3-(3-methoxyphenoxy)-4-methylpentyl)piperidin-4-yl)-2-oxoindolin-3-yl)-N-methylacetamide
CAS No.:1616852-22-2
Molecular Formula:C₃₀H₄₁N₃O₅
Molecular Weight:523.673
Hs Code.:

Synonyms:2-(3-methoxy-1-(1-(3-(3-methoxyphenoxy)-4-methylpentyl)piperidin-4-yl)-2-oxoindolin-3-yl)-N-methylacetamide

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Chemical Property of 2-(3-methoxy-1-(1-(3-(3-methoxyphenoxy)-4-methylpentyl)piperidin-4-yl)-2-oxoindolin-3-yl)-N-methylacetamide

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Technology Process of 2-(3-methoxy-1-(1-(3-(3-methoxyphenoxy)-4-methylpentyl)piperidin-4-yl)-2-oxoindolin-3-yl)-N-methylacetamide

There total 15 articles about 2-(3-methoxy-1-(1-(3-(3-methoxyphenoxy)-4-methylpentyl)piperidin-4-yl)-2-oxoindolin-3-yl)-N-methylacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1616852-20-0
2-(1-(1-(3-(2-chloro-5-methoxyphenoxy)-4-methylpentyl)piperidin-4-yl)-3-methoxy-2-oxoindolin-3-yl)-N-methylacetamide

: 1616852-22-2
2-(3-methoxy-1-(1-(3-(3-methoxyphenoxy)-4-methylpentyl)piperidin-4-yl)-2-oxoindolin-3-yl)-N-methylacetamide

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In methanol; at 20 ℃;

Reference yield:

: 18113-04-7
2-chloro-5-methoxy-phenol

: 1616852-22-2
2-(3-methoxy-1-(1-(3-(3-methoxyphenoxy)-4-methylpentyl)piperidin-4-yl)-2-oxoindolin-3-yl)-N-methylacetamide

Guidance literature:: Multi-step reaction with 4 steps

1: caesium carbonate / dimethyl sulfoxide / 100 °C

2: triethylamine / dichloromethane / 0.17 h / 0 - 20 °C

3: sodium iodide; caesium carbonate / mineral oil; acetonitrile / 5 h / 80 °C

4: hydrogen; palladium 10% on activated carbon / methanol / 20 °C

With palladium 10% on activated carbon; hydrogen; caesium carbonate; triethylamine; sodium iodide; In methanol; dichloromethane; dimethyl sulfoxide; acetonitrile; mineral oil;

Reference yield:

: 150-19-6
O-methylresorcine

: 1616852-22-2
2-(3-methoxy-1-(1-(3-(3-methoxyphenoxy)-4-methylpentyl)piperidin-4-yl)-2-oxoindolin-3-yl)-N-methylacetamide

Guidance literature:: Multi-step reaction with 5 steps

1: thionyl chloride / diethyl ether / 2 h / 0 - 20 °C

2: caesium carbonate / dimethyl sulfoxide / 100 °C

3: triethylamine / dichloromethane / 0.17 h / 0 - 20 °C

4: sodium iodide; caesium carbonate / mineral oil; acetonitrile / 5 h / 80 °C

5: hydrogen; palladium 10% on activated carbon / methanol / 20 °C

With thionyl chloride; palladium 10% on activated carbon; hydrogen; caesium carbonate; triethylamine; sodium iodide; In methanol; diethyl ether; dichloromethane; dimethyl sulfoxide; acetonitrile; mineral oil;