2-(phenoxyacetyl)-N-phenylhydrazinecarbothioamide

Base Information

Chemical Name:2-(phenoxyacetyl)-N-phenylhydrazinecarbothioamide
CAS No.:18233-67-5
Molecular Formula:C₁₅H₁₅N₃O₂S
Molecular Weight:301.369
Hs Code.:
European Community (EC) Number:657-443-3
Nikkaji Number:J1.261.698H

Synonyms:2-(phenoxyacetyl)-N-phenylhydrazinecarbothioamide;ZINC00122726;AKOS003235340;1-phenoxyacetyl-4-phenylthiosemicarbazide

Suppliers and Price of 2-(phenoxyacetyl)-N-phenylhydrazinecarbothioamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2-(phenoxyacetyl)-N-phenylhydrazinecarbothioamide

Chemical Property:

XLogP3:2.7
Hydrogen Bond Donor Count:3
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:4
Exact Mass:301.08849790
Heavy Atom Count:21
Complexity:340

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)NC(=S)NNC(=O)COC2=CC=CC=C2

Technology Process of 2-(phenoxyacetyl)-N-phenylhydrazinecarbothioamide

There total 4 articles about 2-(phenoxyacetyl)-N-phenylhydrazinecarbothioamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 103-72-0
phenyl isothiocyanate

: 4664-55-5
phenoxyacetyl hydrazine

: 18233-67-5
2-(2-phenoxyacetyl)-N-phenylhydrazinecarbothioamide

Guidance literature:: at 45 - 50 ℃; for 12h;

Reference yield:

: 2555-49-9
phenoxyacetic acid ethyl ester

: 18233-67-5
2-(2-phenoxyacetyl)-N-phenylhydrazinecarbothioamide

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine hydrate / ethanol / 3 h / Reflux

2: ethanol / 1 h / Reflux

With hydrazine hydrate; In ethanol;
DOI:10.1021/jm3013213

Reference yield:

: 122-59-8
2-phenoxyacetic acid

: 18233-67-5
2-(2-phenoxyacetyl)-N-phenylhydrazinecarbothioamide

Guidance literature:: Multi-step reaction with 3 steps

1: toluene-4-sulfonic acid / 3 h / Reflux

2: hydrazine hydrate / ethanol / 3 h / Reflux

3: ethanol / 1 h / Reflux

With toluene-4-sulfonic acid; hydrazine hydrate; In ethanol;
DOI:10.1021/jm3013213