perfluorophenyl-9-bora-perfluorofluorene

Base Information

Chemical Name:perfluorophenyl-9-bora-perfluorofluorene
CAS No.:324766-65-6
Molecular Formula:C₁₈BF₁₃
Molecular Weight:473.988
Hs Code.:

Synonyms:perfluorophenyl-9-bora-perfluorofluorene

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Chemical Property of perfluorophenyl-9-bora-perfluorofluorene

Chemical Property:

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Technology Process of perfluorophenyl-9-bora-perfluorofluorene

There total 2 articles about perfluorophenyl-9-bora-perfluorofluorene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 830-48-8
dichloro(pentafluorophenyl)borane

: 17235-00-6
dimethyl 2,2'-(octafluoro biphenyl) stannane

: 753-73-1
dimethyltin dichloride

: 324766-65-6
perfluorophenyl-9-bora-perfluorofluorene

Guidance literature:: In not given;
DOI:10.1021/ja005607u

Reference yield:

: 5576-19-2
2,2'-dibromooctafluorobiphenyl

: 830-48-8
dichloro(pentafluorophenyl)borane

: 324766-65-6
perfluorophenyl-9-bora-perfluorofluorene

Guidance literature:: 2,2'-dibromooctafluorobiphenyl; With n-butyllithium; In diethyl ether; hexane; at -78 ℃; for 2h;

With dimethyltin dichloride; In diethyl ether; hexane; at -78 - 20 ℃;

dichloro(pentafluorophenyl)borane; In benzene; at 70 ℃; for 168h; Further stages.;
DOI:10.1021/ja005607u

Reference yield: 100.0%

: 109-99-9,24979-97-3,77392-70-2
tetrahydrofuran

: 324766-65-6
perfluorophenyl-9-bora-perfluorofluorene

: 892965-05-8
(C₁₂F₈)(C₆F₅)B(OC₄H₈)

Guidance literature:: In dichloromethane; under Ar atm. on fluorinated 9-borafluorene at -78°C CH2Cl2 was condensed and stirred, THF was condensed, warmed to room temp. and stirred for 30 min; solvent was removed in vacuo; elem. anal.;
DOI:10.1139/v05-240