1-benzhydryl-3-(2-benzoyloxyethyl)-5-(2-chlorophenyl)-2-cyanoiminoimidazolidine

Base Information

Chemical Name:1-benzhydryl-3-(2-benzoyloxyethyl)-5-(2-chlorophenyl)-2-cyanoiminoimidazolidine
CAS No.:103866-02-0
Molecular Formula:C₃₂H₂₇ClN₄O₂
Molecular Weight:535.045
Hs Code.:

Synonyms:1-benzhydryl-3-(2-benzoyloxyethyl)-5-(2-chlorophenyl)-2-cyanoiminoimidazolidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-benzhydryl-3-(2-benzoyloxyethyl)-5-(2-chlorophenyl)-2-cyanoiminoimidazolidine

Chemical Property:

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Technology Process of 1-benzhydryl-3-(2-benzoyloxyethyl)-5-(2-chlorophenyl)-2-cyanoiminoimidazolidine

There total 5 articles about 1-benzhydryl-3-(2-benzoyloxyethyl)-5-(2-chlorophenyl)-2-cyanoiminoimidazolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 39252-69-2
2-iodoethyl benzoate

: 103865-99-2
1-benzhydryl-5-(2-chlorophenyl)-2-cyanoiminoimidazolidine

: 103866-02-0
1-benzhydryl-3-(2-benzoyloxyethyl)-5-(2-chlorophenyl)-2-cyanoiminoimidazolidine

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; 1.) RT, 1 h; 2.) 5 h;
DOI:10.1248/cpb.33.2838

Reference yield:

: 89-98-5
2-chloro-benzaldehyde

: 103866-02-0
1-benzhydryl-3-(2-benzoyloxyethyl)-5-(2-chlorophenyl)-2-cyanoiminoimidazolidine

Guidance literature:: Multi-step reaction with 4 steps

1: 85 percent / methanol; H₂O / 5 h / Ambient temperature

2: 92 percent / LiAlH₄ / diethyl ether / 1.) 0-10 deg C, 5 h; 2.) RT, overnight

3: 48 percent / 1.) 100-120 deg C, 30 min; 2.) 190-210 deg C, 30 min

4: 80 percent / 50 percent NaH / dimethylformamide / 1.) RT, 1 h; 2.) 5 h

With lithium aluminium tetrahydride; sodium hydride; In methanol; diethyl ether; water; N,N-dimethyl-formamide;
DOI:10.1248/cpb.33.2838

Reference yield:

: 5267-34-5
aminodiphenylmethane hydrochloride

: 103866-02-0
1-benzhydryl-3-(2-benzoyloxyethyl)-5-(2-chlorophenyl)-2-cyanoiminoimidazolidine

Guidance literature:: Multi-step reaction with 4 steps

1: 85 percent / methanol; H₂O / 5 h / Ambient temperature

2: 92 percent / LiAlH₄ / diethyl ether / 1.) 0-10 deg C, 5 h; 2.) RT, overnight

3: 48 percent / 1.) 100-120 deg C, 30 min; 2.) 190-210 deg C, 30 min

4: 80 percent / 50 percent NaH / dimethylformamide / 1.) RT, 1 h; 2.) 5 h

With lithium aluminium tetrahydride; sodium hydride; In methanol; diethyl ether; water; N,N-dimethyl-formamide;
DOI:10.1248/cpb.33.2838