1,8-bis(2-hydroxy-3,5-di-tert-butylbenzyl)-4,11-dimethyl-1,4,8,11-tetraazacyclotetradecane

Base Information

Chemical Name:1,8-bis(2-hydroxy-3,5-di-tert-butylbenzyl)-4,11-dimethyl-1,4,8,11-tetraazacyclotetradecane
CAS No.:1428144-91-5
Molecular Formula:C₄₂H₇₂N₄O₂
Molecular Weight:665.059
Hs Code.:

Synonyms:1,8-bis(2-hydroxy-3,5-di-tert-butylbenzyl)-4,11-dimethyl-1,4,8,11-tetraazacyclotetradecane

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Chemical Property of 1,8-bis(2-hydroxy-3,5-di-tert-butylbenzyl)-4,11-dimethyl-1,4,8,11-tetraazacyclotetradecane

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Technology Process of 1,8-bis(2-hydroxy-3,5-di-tert-butylbenzyl)-4,11-dimethyl-1,4,8,11-tetraazacyclotetradecane

There total 1 articles about 1,8-bis(2-hydroxy-3,5-di-tert-butylbenzyl)-4,11-dimethyl-1,4,8,11-tetraazacyclotetradecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 96-76-4
2,4-di-tert-Butylphenol

: 214078-92-9
1,8-Dimethyl-1,4,8,11-tetraazacyclotetradecane

: 1428144-91-5
1,8-bis(2-hydroxy-3,5-di-tert-butylbenzyl)-4,11-dimethyl-1,4,8,11-tetraazacyclotetradecane

Guidance literature:: formaldehyd; 1,8-Dimethyl-1,4,8,11-tetraazacyclotetradecane; In methanol; water; for 2h; Inert atmosphere; Reflux;

2,4-di-tert-Butylphenol; In methanol; water; Inert atmosphere; Reflux;
DOI:10.1016/j.jorganchem.2012.12.026

Reference yield:

: 1428144-91-5
1,8-bis(2-hydroxy-3,5-di-tert-butylbenzyl)-4,11-dimethyl-1,4,8,11-tetraazacyclotetradecane

: C₄₂H₇₀N₄O₂^(2-)*2K⁽¹⁺⁾

Guidance literature:: With potassium hydride; In tetrahydrofuran; at 20 ℃; for 16h; Inert atmosphere; Schlenk technique;
DOI:10.1039/c5dt04647e