2-Nitro-4-methoxycarbonylphenyl 2-nitro-5-benzyloxyphenyl sulfide

Base Information

Chemical Name:2-Nitro-4-methoxycarbonylphenyl 2-nitro-5-benzyloxyphenyl sulfide
CAS No.:111012-37-4
Molecular Formula:C₂₁H₁₆N₂O₇S
Molecular Weight:440.433
Hs Code.:

Synonyms:2-Nitro-4-methoxycarbonylphenyl 2-nitro-5-benzyloxyphenyl sulfide

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Chemical Property of 2-Nitro-4-methoxycarbonylphenyl 2-nitro-5-benzyloxyphenyl sulfide

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Technology Process of 2-Nitro-4-methoxycarbonylphenyl 2-nitro-5-benzyloxyphenyl sulfide

There total 5 articles about 2-Nitro-4-methoxycarbonylphenyl 2-nitro-5-benzyloxyphenyl sulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 2363-16-8
methyl 4-bromo-3-nitrobenzoate

: 111012-36-3
2-Nitro-5-benzyloxythiophenol

: 111012-37-4
2-Nitro-4-methoxycarbonylphenyl 2-nitro-5-benzyloxyphenyl sulfide

Guidance literature:: With triethylamine; In N,N-dimethyl-formamide; for 0.25h; Ambient temperature;

Reference yield:

: 5281-18-5
benzaldehyde, hydrazone

: 111012-37-4
2-Nitro-4-methoxycarbonylphenyl 2-nitro-5-benzyloxyphenyl sulfide

Guidance literature:: Multi-step reaction with 5 steps

1: mercuric oxide / pentane / 1 h

2: pentane; diethyl ether

3: 81 percent / Na₂S, S / aq. ethanol / 2 h / Heating

4: 73 percent / ethanethiol, aq. KOH / acetone; H₂O / 0.5 h / 10 - 15 °C

5: 90 percent / triethylamine / dimethylformamide / 0.25 h / Ambient temperature

With sodium sulfide; potassium hydroxide; triethylamine; ethanethiol; mercury(II) oxide; In diethyl ether; ethanol; water; N,N-dimethyl-formamide; acetone; pentane;

Reference yield:

: 50545-45-4
2-chloro-1-nitro-4-phenylmethoxybenzene

: 111012-37-4
2-Nitro-4-methoxycarbonylphenyl 2-nitro-5-benzyloxyphenyl sulfide

Guidance literature:: Multi-step reaction with 3 steps

1: 81 percent / Na₂S, S / aq. ethanol / 2 h / Heating

2: 73 percent / ethanethiol, aq. KOH / acetone; H₂O / 0.5 h / 10 - 15 °C

3: 90 percent / triethylamine / dimethylformamide / 0.25 h / Ambient temperature

With sodium sulfide; potassium hydroxide; triethylamine; ethanethiol; In ethanol; water; N,N-dimethyl-formamide; acetone;