Technology Process of C34H39N3O7S
There total 4 articles about C34H39N3O7S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tetrakis(triphenylphosphine) palladium(0); N-methylaniline;
In
tetrahydrofuran;
at 20 ℃;
for 2.5h;
Inert atmosphere;
DOI:10.1002/anie.201303390
- Guidance literature:
-
Multi-step reaction with 5 steps
1: trifluoroacetic acid / 0.5 h / Inert atmosphere
2: trifluoroacetic acid / Inert atmosphere
3: mercaptoacetic acid; lithium hydroxide / N,N-dimethyl-formamide / 1.5 h / 20 °C / Inert atmosphere
4: triethylamine; trichlorophosphate / dichloromethane / 13.5 h / 0 °C / Inert atmosphere
5: N-methylaniline; tetrakis(triphenylphosphine) palladium(0) / tetrahydrofuran / 2.5 h / 20 °C / Inert atmosphere
With
tetrakis(triphenylphosphine) palladium(0); mercaptoacetic acid; triethylamine; N-methylaniline; trifluoroacetic acid; lithium hydroxide; trichlorophosphate;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/anie.201303390
- Guidance literature:
-
Multi-step reaction with 3 steps
1: mercaptoacetic acid; lithium hydroxide / N,N-dimethyl-formamide / 1.5 h / 20 °C / Inert atmosphere
2: triethylamine; trichlorophosphate / dichloromethane / 13.5 h / 0 °C / Inert atmosphere
3: N-methylaniline; tetrakis(triphenylphosphine) palladium(0) / tetrahydrofuran / 2.5 h / 20 °C / Inert atmosphere
With
tetrakis(triphenylphosphine) palladium(0); mercaptoacetic acid; triethylamine; N-methylaniline; lithium hydroxide; trichlorophosphate;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/anie.201303390
