N,N'-bis(ethyl-4,6-O-benzylidene-2-deoxy-3-O-triethylsilyl-1-thio-β-D-glucopyranosid-2-yl)dimethylmalonamide

Base Information

Chemical Name:N,N'-bis(ethyl-4,6-O-benzylidene-2-deoxy-3-O-triethylsilyl-1-thio-β-D-glucopyranosid-2-yl)dimethylmalonamide
CAS No.:1062081-05-3
Molecular Formula:C₄₇H₇₄N₂O₁₀S₂Si₂
Molecular Weight:947.415
Hs Code.:

Synonyms:N,N'-bis(ethyl-4,6-O-benzylidene-2-deoxy-3-O-triethylsilyl-1-thio-β-D-glucopyranosid-2-yl)dimethylmalonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N'-bis(ethyl-4,6-O-benzylidene-2-deoxy-3-O-triethylsilyl-1-thio-β-D-glucopyranosid-2-yl)dimethylmalonamide

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Technology Process of N,N'-bis(ethyl-4,6-O-benzylidene-2-deoxy-3-O-triethylsilyl-1-thio-β-D-glucopyranosid-2-yl)dimethylmalonamide

There total 1 articles about N,N'-bis(ethyl-4,6-O-benzylidene-2-deoxy-3-O-triethylsilyl-1-thio-β-D-glucopyranosid-2-yl)dimethylmalonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1062080-87-8
N,N'-bis(ethyl-4,6-O-benzylidene-2-deoxy-1-thio-β-D-glucopyranosid-2-yl)dimethylmalonamide

: 79271-56-0
triethylsilyl trifluoromethyl sulfonate

: 1062081-05-3
N,N'-bis(ethyl-4,6-O-benzylidene-2-deoxy-3-O-triethylsilyl-1-thio-β-D-glucopyranosid-2-yl)dimethylmalonamide

Guidance literature:: With triethylamine; In dichloromethane; at -78 - 20 ℃; for 16h;
DOI:10.1055/S-2008-1078419

Reference yield: 85.0%

: 1062081-05-3
N,N'-bis(ethyl-4,6-O-benzylidene-2-deoxy-3-O-triethylsilyl-1-thio-β-D-glucopyranosid-2-yl)dimethylmalonamide

: 1062081-14-4
C₄₃H₆₂N₂O₁₀Si₂

Guidance literature:: With N-iodo-succinimide; trifluorormethanesulfonic acid; In dichloromethane; at -30 ℃; for 1h; Molecular sieve; Inert atmosphere;
DOI:10.1055/S-2008-1078419

Reference yield: 85.0%

: 1062081-05-3
N,N'-bis(ethyl-4,6-O-benzylidene-2-deoxy-3-O-triethylsilyl-1-thio-β-D-glucopyranosid-2-yl)dimethylmalonamide

: C₄₃H₆₂N₂O₈Si₂

Guidance literature:: N,N'-bis(ethyl-4,6-O-benzylidene-2-deoxy-3-O-triethylsilyl-1-thio-β-D-glucopyranosid-2-yl)dimethylmalonamide; In dichloromethane; for 1h; Molecular sieve; Inert atmosphere;

With N-iodo-succinimide; trifluorormethanesulfonic acid; In dichloromethane; at -30 ℃; for 1h; Inert atmosphere; Molecular sieve;
DOI:10.1002/ejoc.200801035