N-2-<(2-acetamido-4-thiazolyl)ethyl>-3,5-diiodo-4-methoxyphenylacetamido

Base Information

Chemical Name:N-2-<(2-acetamido-4-thiazolyl)ethyl>-3,5-diiodo-4-methoxyphenylacetamido
CAS No.:221658-95-3
Molecular Formula:C₁₆H₁₇I₂N₃O₃S
Molecular Weight:585.204
Hs Code.:

Synonyms:N-2-<(2-acetamido-4-thiazolyl)ethyl>-3,5-diiodo-4-methoxyphenylacetamido

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Chemical Property of N-2-<(2-acetamido-4-thiazolyl)ethyl>-3,5-diiodo-4-methoxyphenylacetamido

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Technology Process of N-2-<(2-acetamido-4-thiazolyl)ethyl>-3,5-diiodo-4-methoxyphenylacetamido

There total 5 articles about N-2-<(2-acetamido-4-thiazolyl)ethyl>-3,5-diiodo-4-methoxyphenylacetamido which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 108-24-7
acetic anhydride

: 221658-93-1
N-2-<(2-amino-4-thiazolyl)ethyl>-3,5-diiodo-4-methoxyphenylacetamido

: 221658-95-3
N-2-<(2-acetamido-4-thiazolyl)ethyl>-3,5-diiodo-4-methoxyphenylacetamido

Guidance literature:: In acetonitrile; benzene; for 2.5h; Heating;
DOI:10.1021/jm990012z

Reference yield:

: 95914-09-3
2-[2-(2-amino-1,3-thiazol-4-yl)ethyl]-1H-isoindole-1,3(2H)-dione hydrobromide

: 221658-95-3
N-2-<(2-acetamido-4-thiazolyl)ethyl>-3,5-diiodo-4-methoxyphenylacetamido

Guidance literature:: Multi-step reaction with 3 steps

1: 30 percent aq. HBr / Heating

2: NaOH / CHCl₃ / 1.5 h / Ambient temperature

3: 92 percent / acetonitrile; benzene / 2.5 h / Heating

With sodium hydroxide; hydrogen bromide; In chloroform; acetonitrile; benzene;
DOI:10.1021/jm990012z

Reference yield:

: 221660-62-4
3,5-diiodo-4-methoxyphenylacetyl chloride

: 221658-95-3
N-2-<(2-acetamido-4-thiazolyl)ethyl>-3,5-diiodo-4-methoxyphenylacetamido

Guidance literature:: Multi-step reaction with 2 steps

1: NaOH / CHCl₃ / 1.5 h / Ambient temperature

2: 92 percent / acetonitrile; benzene / 2.5 h / Heating

With sodium hydroxide; In chloroform; acetonitrile; benzene;
DOI:10.1021/jm990012z