3-bromo-5-iodobenzoylazide

Base Information

• Chemical Name: 3-bromo-5-iodobenzoylazide
• CAS No.: 915413-41-1
• Molecular Formula: C₇H₃BrIN₃O
• Molecular Weight: 351.929

Synonyms:3-bromo-5-iodobenzoylazide

Chemical Property of 3-bromo-5-iodobenzoylazide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-bromo-5-iodobenzoylazide

There total 1 articles about 3-bromo-5-iodobenzoylazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

3-bromo-5-iodo-benzoic acid (188815-32-9) → 3-bromo-5-iodobenzoylazide (915413-41-1)

Guidance literature:

With diphenyl phosphoryl azide; N-ethyl-N,N-diisopropylamine; In methanol; at 20 ℃; for 12h;

Reference yield: 100.0%

3-bromo-5-iodobenzoylazide (915413-41-1) → 1-bromo-3-iodo-5-isocyanato-benzene

Guidance literature:

In toluene; for 3.5h; Reflux;

DOI:10.1002/ejoc.201900362

Reference yield: 99.0%

3-bromo-5-iodobenzoylazide (915413-41-1) + tert-butyl alcohol (75-65-0) → (3-bromo-5-iodophenyl)carbamic acid tert-butyl ester (915413-42-2)

Guidance literature:

In toluene; for 2h; Heating / reflux;

upstream raw materials:

3-bromo-5-iodo-benzoic acid

Downstream raw materials:

(3-bromo-5-iodophenyl)carbamic acid tert-butyl ester

N-(3-bromo-5-iodophenyl)methanesulfonamide

N-(3-bromo-5-iodophenyl)acetamide

N-(3-bromo-5-(6-methoxypyridin-3-yl)phenyl)acetamide

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