4-methoxyphenyl (methyl 4,7,8,9-tetra-O-acetyl-3,5-dideoxy-5-(2,2,2-trichloroethoxycarbamoyl)-D-glycero-α-D-galacto-2-nonulopyranosylonate)-(2→6)-2,3-di-O-benzyl-β-D-galactopyranoside

Base Information

Chemical Name:4-methoxyphenyl (methyl 4,7,8,9-tetra-O-acetyl-3,5-dideoxy-5-(2,2,2-trichloroethoxycarbamoyl)-D-glycero-α-D-galacto-2-nonulopyranosylonate)-(2→6)-2,3-di-O-benzyl-β-D-galactopyranoside
CAS No.:1404292-17-6
Molecular Formula:C₄₈H₅₆Cl₃NO₂₀
Molecular Weight:1073.33
Hs Code.:

4-methoxyphenyl (methyl 4,7,8,9-tetra-O-acetyl-3,5-dideoxy-5-(2,2,2-trichloroethoxycarbamoyl)-D-glycero-α-D-galacto-2-nonulopyranosylonate)-(2→6)-2,3-di-O-benzyl-β-D-galactopyranoside

Synonyms:4-methoxyphenyl (methyl 4,7,8,9-tetra-O-acetyl-3,5-dideoxy-5-(2,2,2-trichloroethoxycarbamoyl)-D-glycero-α-D-galacto-2-nonulopyranosylonate)-(2→6)-2,3-di-O-benzyl-β-D-galactopyranoside

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Chemical Property of 4-methoxyphenyl (methyl 4,7,8,9-tetra-O-acetyl-3,5-dideoxy-5-(2,2,2-trichloroethoxycarbamoyl)-D-glycero-α-D-galacto-2-nonulopyranosylonate)-(2→6)-2,3-di-O-benzyl-β-D-galactopyranoside

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Technology Process of 4-methoxyphenyl (methyl 4,7,8,9-tetra-O-acetyl-3,5-dideoxy-5-(2,2,2-trichloroethoxycarbamoyl)-D-glycero-α-D-galacto-2-nonulopyranosylonate)-(2→6)-2,3-di-O-benzyl-β-D-galactopyranoside

There total 1 articles about 4-methoxyphenyl (methyl 4,7,8,9-tetra-O-acetyl-3,5-dideoxy-5-(2,2,2-trichloroethoxycarbamoyl)-D-glycero-α-D-galacto-2-nonulopyranosylonate)-(2→6)-2,3-di-O-benzyl-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 1404292-12-1
C₂₇H₃₀O₇

: Neu₅'Troc

: 4-methoxyphenyl (methyl 4,7,8,9-tetra-O-acetyl-3,5-dideoxy-5-(2,2,2-trichloroethoxycarbamoyl)-D-glycero-β-D-galacto-2-nonulopyranosylonate)-(2→6)-2,3-di-O-benzyl-β-D-galactopyranoside

: 1404292-17-6
4-methoxyphenyl (methyl 4,7,8,9-tetra-O-acetyl-3,5-dideoxy-5-(2,2,2-trichloroethoxycarbamoyl)-D-glycero-α-D-galacto-2-nonulopyranosylonate)-(2→6)-2,3-di-O-benzyl-β-D-galactopyranoside

Guidance literature:: With N-iodo-succinimide; trifluorormethanesulfonic acid; In dichloromethane; at -30 ℃; for 0.75h; Molecular sieve; Inert atmosphere;
DOI:10.3390/molecules17089590

Reference yield:

: 1404292-17-6
4-methoxyphenyl (methyl 4,7,8,9-tetra-O-acetyl-3,5-dideoxy-5-(2,2,2-trichloroethoxycarbamoyl)-D-glycero-α-D-galacto-2-nonulopyranosylonate)-(2→6)-2,3-di-O-benzyl-β-D-galactopyranoside

: C₄₅H₅₅NO₁₈

Guidance literature:: With zinc-copper couple; acetic acid; In dichloromethane; at 40 ℃; for 0.75h; Inert atmosphere;
DOI:10.3390/molecules17089590

Reference yield:

: 1404292-17-6
4-methoxyphenyl (methyl 4,7,8,9-tetra-O-acetyl-3,5-dideoxy-5-(2,2,2-trichloroethoxycarbamoyl)-D-glycero-α-D-galacto-2-nonulopyranosylonate)-(2→6)-2,3-di-O-benzyl-β-D-galactopyranoside

: C₄₂H₄₉NO₂₁

Guidance literature:: Multi-step reaction with 5 steps

1: zinc-copper couple; acetic acid / dichloromethane / 0.75 h / 40 °C / Inert atmosphere

2: pyridine; dmap / 72 h / 0 - 20 °C / Inert atmosphere

3: Pd(OH)2/C; hydrogen / 1,4-dioxane / 0.75 h / 20 °C / Inert atmosphere

4: pyridine; dmap / 9 h / 0 - 20 °C / Inert atmosphere

5: ammonium cerium (IV) nitrate; water / acetonitrile; toluene / 2 h / 20 °C / Inert atmosphere

With pyridine; dmap; ammonium cerium (IV) nitrate; Pd(OH)2/C; zinc-copper couple; water; hydrogen; acetic acid; In 1,4-dioxane; dichloromethane; toluene; acetonitrile;
DOI:10.3390/molecules17089590