4-methoxyphenyl (methyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosylonate)-(2→6)-4-O-acetyl-2,3-di-O-benzoyl-β-D-galactopyranoside

Base Information

Chemical Name:4-methoxyphenyl (methyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosylonate)-(2→6)-4-O-acetyl-2,3-di-O-benzoyl-β-D-galactopyranoside
CAS No.:1404292-27-8
Molecular Formula:C₄₉H₅₅NO₂₂
Molecular Weight:1009.97
Hs Code.:

4-methoxyphenyl (methyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosylonate)-(2→6)-4-O-acetyl-2,3-di-O-benzoyl-β-D-galactopyranoside

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Chemical Property of 4-methoxyphenyl (methyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosylonate)-(2→6)-4-O-acetyl-2,3-di-O-benzoyl-β-D-galactopyranoside

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Technology Process of 4-methoxyphenyl (methyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosylonate)-(2→6)-4-O-acetyl-2,3-di-O-benzoyl-β-D-galactopyranoside

There total 5 articles about 4-methoxyphenyl (methyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosylonate)-(2→6)-4-O-acetyl-2,3-di-O-benzoyl-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1404292-12-1
C₂₇H₃₀O₇

: 1404292-27-8
4-methoxyphenyl (methyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosylonate)-(2→6)-4-O-acetyl-2,3-di-O-benzoyl-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 5 steps

1: N-iodo-succinimide; trifluorormethanesulfonic acid / dichloromethane / 0.75 h / -30 °C / Molecular sieve; Inert atmosphere

2: zinc-copper couple; acetic acid / dichloromethane / 0.75 h / 40 °C / Inert atmosphere

3: pyridine; dmap / 72 h / 0 - 20 °C / Inert atmosphere

4: Pd(OH)2/C; hydrogen / 1,4-dioxane / 0.75 h / 20 °C / Inert atmosphere

5: pyridine; dmap / 9 h / 0 - 20 °C / Inert atmosphere

With pyridine; dmap; N-iodo-succinimide; trifluorormethanesulfonic acid; Pd(OH)2/C; zinc-copper couple; hydrogen; acetic acid; In 1,4-dioxane; dichloromethane;
DOI:10.3390/molecules17089590

Reference yield:

: C₄₅H₅₅NO₁₈

: 1404292-27-8
4-methoxyphenyl (methyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosylonate)-(2→6)-4-O-acetyl-2,3-di-O-benzoyl-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine; dmap / 72 h / 0 - 20 °C / Inert atmosphere

2: Pd(OH)2/C; hydrogen / 1,4-dioxane / 0.75 h / 20 °C / Inert atmosphere

3: pyridine; dmap / 9 h / 0 - 20 °C / Inert atmosphere

With pyridine; dmap; Pd(OH)2/C; hydrogen; In 1,4-dioxane;
DOI:10.3390/molecules17089590

Reference yield:

: 1404292-17-6
4-methoxyphenyl (methyl 4,7,8,9-tetra-O-acetyl-3,5-dideoxy-5-(2,2,2-trichloroethoxycarbamoyl)-D-glycero-α-D-galacto-2-nonulopyranosylonate)-(2→6)-2,3-di-O-benzyl-β-D-galactopyranoside

: 1404292-27-8
4-methoxyphenyl (methyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosylonate)-(2→6)-4-O-acetyl-2,3-di-O-benzoyl-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: zinc-copper couple; acetic acid / dichloromethane / 0.75 h / 40 °C / Inert atmosphere

2: pyridine; dmap / 72 h / 0 - 20 °C / Inert atmosphere

3: Pd(OH)2/C; hydrogen / 1,4-dioxane / 0.75 h / 20 °C / Inert atmosphere

4: pyridine; dmap / 9 h / 0 - 20 °C / Inert atmosphere

With pyridine; dmap; Pd(OH)2/C; zinc-copper couple; hydrogen; acetic acid; In 1,4-dioxane; dichloromethane;
DOI:10.3390/molecules17089590