methyl (phenyl 5-tert-butoxycarbonylamino-3,5-dideoxy-2-thio-D-glycero-α-D-galacto-2-nonulopyranosid)uronate

Base Information

• Chemical Name: methyl (phenyl 5-tert-butoxycarbonylamino-3,5-dideoxy-2-thio-D-glycero-α-D-galacto-2-nonulopyranosid)uronate
• CAS No.: 1046456-64-7
• Molecular Formula: C₂₁H₃₁NO₉S
• Molecular Weight: 473.544

Synonyms:methyl (phenyl 5-tert-butoxycarbonylamino-3,5-dideoxy-2-thio-D-glycero-α-D-galacto-2-nonulopyranosid)uronate

Chemical Property of methyl (phenyl 5-tert-butoxycarbonylamino-3,5-dideoxy-2-thio-D-glycero-α-D-galacto-2-nonulopyranosid)uronate

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Technology Process of methyl (phenyl 5-tert-butoxycarbonylamino-3,5-dideoxy-2-thio-D-glycero-α-D-galacto-2-nonulopyranosid)uronate

There total 1 articles about methyl (phenyl 5-tert-butoxycarbonylamino-3,5-dideoxy-2-thio-D-glycero-α-D-galacto-2-nonulopyranosid)uronate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C29H39NO13S (432023-46-6) → methyl (phenyl 5-tert-butoxycarbonylamino-3,5-dideoxy-2-thio-D-glycero-α-D-galacto-2-nonulopyranosid)uronate (1046456-64-7)

Guidance literature:

With sodium methylate; In methanol; at 20 ℃; for 11h;

DOI:10.1016/j.carres.2008.05.005

Reference yield: 96.0%

methyl (phenyl 5-tert-butoxycarbonylamino-3,5-dideoxy-2-thio-D-glycero-α-D-galacto-2-nonulopyranosid)uronate (1046456-64-7) + 2,2-dimethoxy-propane (77-76-9) → methyl (phenyl 5-tert-butoxycarbonylamino-8,9-isopropylidene-3,5-dideoxy-2-thio-D-glycero-α-D-galacto-2-nonulopyranosid)uronate (1046456-65-8)

Guidance literature:

With camphor-10-sulfonic acid; In acetonitrile; at 20 ℃; for 0.166667h;

DOI:10.1016/j.carres.2008.05.005

Reference yield:

methyl (phenyl 5-tert-butoxycarbonylamino-3,5-dideoxy-2-thio-D-glycero-α-D-galacto-2-nonulopyranosid)uronate (1046456-64-7) → thiophenyl 5-N-tert-butoxycarbonyl-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosylonic acid (1160107-00-5)

Guidance literature:

With lithium hydroxide; In methanol; water; at 20 ℃;

DOI:10.1021/jm801609s

upstream raw materials:

C₂₉H₃₉NO₁₃S

Downstream raw materials:

methyl (phenyl 5-tert-butoxycarbonylamino-8,9-isopropylidene-3,5-dideoxy-2-thio-D-glycero-α-D-galacto-2-nonulopyranosid)uronate

thiophenyl 5-N-tert-butoxycarbonyl-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosylonic acid

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