(1-(2-fluorobenzyl)-1H-1,2,3-triazol-4-yl)methyl piperazine-1-carbodithioate

Base Information

Chemical Name:(1-(2-fluorobenzyl)-1H-1,2,3-triazol-4-yl)methyl piperazine-1-carbodithioate
CAS No.:1418150-29-4
Molecular Formula:C₁₅H₁₈FN₅S₂
Molecular Weight:351.472
Hs Code.:

Synonyms:(1-(2-fluorobenzyl)-1H-1,2,3-triazol-4-yl)methyl piperazine-1-carbodithioate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1-(2-fluorobenzyl)-1H-1,2,3-triazol-4-yl)methyl piperazine-1-carbodithioate

Chemical Property:

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Technology Process of (1-(2-fluorobenzyl)-1H-1,2,3-triazol-4-yl)methyl piperazine-1-carbodithioate

There total 3 articles about (1-(2-fluorobenzyl)-1H-1,2,3-triazol-4-yl)methyl piperazine-1-carbodithioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.7%

: 1418150-12-5
tert-butyl 4-(((1-(2-fluorobenzyl)-1H-1,2,3-triazol-4-yl)methylthio)carbonothioyl)piperazine-1-carboxylate

: 1418150-29-4
(1-(2-fluorobenzyl)-1H-1,2,3-triazol-4-yl)methyl piperazine-1-carbodithioate

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 0 - 20 ℃; for 8h;
DOI:10.1021/jm401002r

Reference yield:

: 1418150-39-6
tert-butyl-4-((prop-2-yn-1-ylthio)carbonothioyl)piperazine-1-carboxylate

: 1418150-29-4
(1-(2-fluorobenzyl)-1H-1,2,3-triazol-4-yl)methyl piperazine-1-carbodithioate

Guidance literature:: Multi-step reaction with 2 steps

1: copper(ll) sulfate pentahydrate; sodium L-ascorbate / tetrahydrofuran; water / 20 °C

2: trifluoroacetic acid / dichloromethane / 0 - 20 °C

With copper(ll) sulfate pentahydrate; sodium L-ascorbate; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; water;
DOI:10.1016/j.ejmech.2012.12.046

Reference yield:

: 773024-43-4
C₁₀H₁₈N₂O₂S₂

: 1418150-29-4
(1-(2-fluorobenzyl)-1H-1,2,3-triazol-4-yl)methyl piperazine-1-carbodithioate

Guidance literature:: Multi-step reaction with 3 steps

1: acetone / 0.5 h / 20 °C

2: copper(ll) sulfate pentahydrate; sodium L-ascorbate / tetrahydrofuran; water / 20 °C

3: trifluoroacetic acid / dichloromethane / 0 - 20 °C

With copper(ll) sulfate pentahydrate; sodium L-ascorbate; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; water; acetone;
DOI:10.1016/j.ejmech.2012.12.046