perfluorophenyl 3-(2-(2-(3-methyl-5-oxo-4,5-dihydro-1H-pyrazol-1-yl)ethoxy)ethoxy)propanoate

Base Information

Chemical Name:perfluorophenyl 3-(2-(2-(3-methyl-5-oxo-4,5-dihydro-1H-pyrazol-1-yl)ethoxy)ethoxy)propanoate
CAS No.:1609643-83-5
Molecular Formula:C₁₇H₁₇F₅N₂O₅
Molecular Weight:424.324
Hs Code.:

Synonyms:perfluorophenyl 3-(2-(2-(3-methyl-5-oxo-4,5-dihydro-1H-pyrazol-1-yl)ethoxy)ethoxy)propanoate

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Chemical Property of perfluorophenyl 3-(2-(2-(3-methyl-5-oxo-4,5-dihydro-1H-pyrazol-1-yl)ethoxy)ethoxy)propanoate

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Technology Process of perfluorophenyl 3-(2-(2-(3-methyl-5-oxo-4,5-dihydro-1H-pyrazol-1-yl)ethoxy)ethoxy)propanoate

There total 6 articles about perfluorophenyl 3-(2-(2-(3-methyl-5-oxo-4,5-dihydro-1H-pyrazol-1-yl)ethoxy)ethoxy)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 771-61-9
2,3,4,5,6-pentafluorophenol

: 1609643-82-4
3-(2-(2-(3-methyl-5-oxo-4,5-dihydro-1H-pyrazol-1-yl)ethoxy)ethoxy)propanoic acid

: 1609643-83-5
perfluorophenyl 3-(2-(2-(3-methyl-5-oxo-4,5-dihydro-1H-pyrazol-1-yl)ethoxy)ethoxy)propanoate

Guidance literature:: With dicyclohexyl-carbodiimide; In ethyl acetate; at 0 - 20 ℃; for 5h;

Reference yield:

: 1491136-22-1
tert-butyl 3-(2-(2-oxoethoxy)ethoxy)propanoate

: 1609643-83-5
perfluorophenyl 3-(2-(2-(3-methyl-5-oxo-4,5-dihydro-1H-pyrazol-1-yl)ethoxy)ethoxy)propanoate

Guidance literature:: Multi-step reaction with 5 steps

1: toluene / 48 h

2: sodium cyanoborohydride; acetic acid / methanol

3: water / 0.75 h

4: acetic acid / 16 h / Reflux

5: dicyclohexyl-carbodiimide / ethyl acetate / 5 h / 0 - 20 °C

With water; sodium cyanoborohydride; acetic acid; dicyclohexyl-carbodiimide; In methanol; ethyl acetate; toluene;

Reference yield:

: 133803-81-3,892154-71-1
2-methyl-2-propanyl 3-[2-(2-hydroxyethoxy)ethoxy]propanoate

: 1609643-83-5
perfluorophenyl 3-(2-(2-(3-methyl-5-oxo-4,5-dihydro-1H-pyrazol-1-yl)ethoxy)ethoxy)propanoate

Guidance literature:: Multi-step reaction with 6 steps

1: Dess-Martin periodane; pyridine / dichloromethane / 3 h

2: toluene / 48 h

3: sodium cyanoborohydride; acetic acid / methanol

4: water / 0.75 h

5: acetic acid / 16 h / Reflux

6: dicyclohexyl-carbodiimide / ethyl acetate / 5 h / 0 - 20 °C

With pyridine; water; sodium cyanoborohydride; Dess-Martin periodane; acetic acid; dicyclohexyl-carbodiimide; In methanol; dichloromethane; ethyl acetate; toluene;