1,1-dimethylethyl cyclopropyl{[2,3-dichloro-5-(2-{[(methyloxy)carbonyl]amino}ethyl)phenyl]methyl}carbamate

Base Information

Chemical Name:1,1-dimethylethyl cyclopropyl{[2,3-dichloro-5-(2-{[(methyloxy)carbonyl]amino}ethyl)phenyl]methyl}carbamate
CAS No.:1229245-80-0
Molecular Formula:C₁₉H₂₆Cl₂N₂O₄
Molecular Weight:417.332
Hs Code.:

Synonyms:1,1-dimethylethyl cyclopropyl{[2,3-dichloro-5-(2-{[(methyloxy)carbonyl]amino}ethyl)phenyl]methyl}carbamate

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Chemical Property of 1,1-dimethylethyl cyclopropyl{[2,3-dichloro-5-(2-{[(methyloxy)carbonyl]amino}ethyl)phenyl]methyl}carbamate

Chemical Property:

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Technology Process of 1,1-dimethylethyl cyclopropyl{[2,3-dichloro-5-(2-{[(methyloxy)carbonyl]amino}ethyl)phenyl]methyl}carbamate

There total 12 articles about 1,1-dimethylethyl cyclopropyl{[2,3-dichloro-5-(2-{[(methyloxy)carbonyl]amino}ethyl)phenyl]methyl}carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1229245-81-1
1,1-dimethylethyl {[5-(2-aminoethyl)-2,3-dichlorophenyl]methyl}cyclopropylcarbamate

: 79-22-1
methyl chloroformate

: 1229245-80-0
1,1-dimethylethyl cyclopropyl{[2,3-dichloro-5-(2-{[(methyloxy)carbonyl]amino}ethyl)phenyl]methyl}carbamate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 - 20 ℃; for 3h;

Reference yield:

: 1229246-37-0
5-bromo-2,3-dichlorobenzaldehyde

: 1229245-80-0
1,1-dimethylethyl cyclopropyl{[2,3-dichloro-5-(2-{[(methyloxy)carbonyl]amino}ethyl)phenyl]methyl}carbamate

Guidance literature:: Multi-step reaction with 11 steps

1.1: magnesium sulfate / dichloromethane / 20 °C

2.1: magnesium sulfate / dichloromethane / 20 °C

3.1: sodium tetrahydroborate / tetrahydrofuran; methanol / 48 h / 20 °C

4.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 3 h / 20 °C

5.1: sodium carbonate; triphenylphosphine / palladium diacetate / propan-1-ol; water; N,N-dimethyl-formamide / 18 h / 90 °C / Inert atmosphere of nitrogen

6.1: ozone / dichloromethane / -78 °C

6.2: 3 h / -78 - 20 °C

7.1: sodium tetrahydroborate / methanol / 2 h / 0 °C

8.1: N-ethyl-N,N-diisopropylamine / 0 - 20 °C

9.1: sodium iodide / dimethyl sulfoxide / 3 h / 20 °C

10.1: sodium tetrahydroborate; cobalt(II) chloride hexahydrate / methanol

11.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 3 h / 0 - 20 °C

With sodium tetrahydroborate; cobalt(II) chloride hexahydrate; sodium carbonate; magnesium sulfate; ozone; N-ethyl-N,N-diisopropylamine; triphenylphosphine; sodium iodide; palladium diacetate; In tetrahydrofuran; methanol; propan-1-ol; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; 5.1: Suzuki Coupling;

Reference yield:

: C₁₀H₈BrCl₂N

: 1229245-80-0
1,1-dimethylethyl cyclopropyl{[2,3-dichloro-5-(2-{[(methyloxy)carbonyl]amino}ethyl)phenyl]methyl}carbamate

Guidance literature:: Multi-step reaction with 9 steps

1.1: sodium tetrahydroborate / tetrahydrofuran; methanol / 48 h / 20 °C

2.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 3 h / 20 °C

3.1: sodium carbonate; triphenylphosphine / palladium diacetate / propan-1-ol; water; N,N-dimethyl-formamide / 18 h / 90 °C / Inert atmosphere of nitrogen

4.1: ozone / dichloromethane / -78 °C

4.2: 3 h / -78 - 20 °C

5.1: sodium tetrahydroborate / methanol / 2 h / 0 °C

6.1: N-ethyl-N,N-diisopropylamine / 0 - 20 °C

7.1: sodium iodide / dimethyl sulfoxide / 3 h / 20 °C

8.1: sodium tetrahydroborate; cobalt(II) chloride hexahydrate / methanol

9.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 3 h / 0 - 20 °C

With sodium tetrahydroborate; cobalt(II) chloride hexahydrate; sodium carbonate; ozone; N-ethyl-N,N-diisopropylamine; triphenylphosphine; sodium iodide; palladium diacetate; In tetrahydrofuran; methanol; propan-1-ol; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; 3.1: Suzuki Coupling;