1,1-dimethylethyl {[5-(2-aminoethyl)-2,3-dichlorophenyl]methyl}cyclopropylcarbamate

Base Information

Chemical Name:1,1-dimethylethyl {[5-(2-aminoethyl)-2,3-dichlorophenyl]methyl}cyclopropylcarbamate
CAS No.:1229245-81-1
Molecular Formula:C₁₇H₂₄Cl₂N₂O₂
Molecular Weight:359.296
Hs Code.:

Synonyms:1,1-dimethylethyl {[5-(2-aminoethyl)-2,3-dichlorophenyl]methyl}cyclopropylcarbamate

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Chemical Property of 1,1-dimethylethyl {[5-(2-aminoethyl)-2,3-dichlorophenyl]methyl}cyclopropylcarbamate

Chemical Property:

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Technology Process of 1,1-dimethylethyl {[5-(2-aminoethyl)-2,3-dichlorophenyl]methyl}cyclopropylcarbamate

There total 11 articles about 1,1-dimethylethyl {[5-(2-aminoethyl)-2,3-dichlorophenyl]methyl}cyclopropylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1229245-82-2
1,1-dimethylethyl cyclopropyl{[2,3-dichloro-5-(cyanomethyl)phenyl]methyl}carbamate

: 1229245-81-1
1,1-dimethylethyl {[5-(2-aminoethyl)-2,3-dichlorophenyl]methyl}cyclopropylcarbamate

Guidance literature:: 1,1-dimethylethyl cyclopropyl{[2,3-dichloro-5-(cyanomethyl)phenyl]methyl}carbamate; With sodium tetrahydroborate; cobalt(II) chloride hexahydrate; In methanol;

With water; sodium hydroxide; In methanol;

Reference yield:

: 1229246-37-0
5-bromo-2,3-dichlorobenzaldehyde

: 1229245-81-1
1,1-dimethylethyl {[5-(2-aminoethyl)-2,3-dichlorophenyl]methyl}cyclopropylcarbamate

Guidance literature:: Multi-step reaction with 10 steps

1.1: magnesium sulfate / dichloromethane / 20 °C

2.1: magnesium sulfate / dichloromethane / 20 °C

3.1: sodium tetrahydroborate / tetrahydrofuran; methanol / 48 h / 20 °C

4.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 3 h / 20 °C

5.1: sodium carbonate; triphenylphosphine / palladium diacetate / propan-1-ol; water; N,N-dimethyl-formamide / 18 h / 90 °C / Inert atmosphere of nitrogen

6.1: ozone / dichloromethane / -78 °C

6.2: 3 h / -78 - 20 °C

7.1: sodium tetrahydroborate / methanol / 2 h / 0 °C

8.1: N-ethyl-N,N-diisopropylamine / 0 - 20 °C

9.1: sodium iodide / dimethyl sulfoxide / 3 h / 20 °C

10.1: sodium tetrahydroborate; cobalt(II) chloride hexahydrate / methanol

With sodium tetrahydroborate; cobalt(II) chloride hexahydrate; sodium carbonate; magnesium sulfate; ozone; N-ethyl-N,N-diisopropylamine; triphenylphosphine; sodium iodide; palladium diacetate; In tetrahydrofuran; methanol; propan-1-ol; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; 5.1: Suzuki Coupling;

Reference yield:

: C₁₀H₈BrCl₂N

: 1229245-81-1
1,1-dimethylethyl {[5-(2-aminoethyl)-2,3-dichlorophenyl]methyl}cyclopropylcarbamate

Guidance literature:: Multi-step reaction with 8 steps

1.1: sodium tetrahydroborate / tetrahydrofuran; methanol / 48 h / 20 °C

2.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 3 h / 20 °C

3.1: sodium carbonate; triphenylphosphine / palladium diacetate / propan-1-ol; water; N,N-dimethyl-formamide / 18 h / 90 °C / Inert atmosphere of nitrogen

4.1: ozone / dichloromethane / -78 °C

4.2: 3 h / -78 - 20 °C

5.1: sodium tetrahydroborate / methanol / 2 h / 0 °C

6.1: N-ethyl-N,N-diisopropylamine / 0 - 20 °C

7.1: sodium iodide / dimethyl sulfoxide / 3 h / 20 °C

8.1: sodium tetrahydroborate; cobalt(II) chloride hexahydrate / methanol

With sodium tetrahydroborate; cobalt(II) chloride hexahydrate; sodium carbonate; ozone; N-ethyl-N,N-diisopropylamine; triphenylphosphine; sodium iodide; palladium diacetate; In tetrahydrofuran; methanol; propan-1-ol; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; 3.1: Suzuki Coupling;