Acetic acid (2R,3R,4S,5R,6R)-3-acetoxy-6-acetoxymethyl-2-(2-{2-[2-(2-azido-ethoxy)-ethoxy]-ethoxy}-acetylamino)-5-((2S,3R,4S,5S,6R)-3,4,5-triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-4-yl ester

Base Information

Chemical Name:Acetic acid (2R,3R,4S,5R,6R)-3-acetoxy-6-acetoxymethyl-2-(2-{2-[2-(2-azido-ethoxy)-ethoxy]-ethoxy}-acetylamino)-5-((2S,3R,4S,5S,6R)-3,4,5-triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-4-yl ester
CAS No.:176167-85-4
Molecular Formula:C₃₄H₅₀N₄O₂₁
Molecular Weight:850.785
Hs Code.:

Acetic acid (2R,3R,4S,5R,6R)-3-acetoxy-6-acetoxymethyl-2-(2-{2-[2-(2-azido-ethoxy)-ethoxy]-ethoxy}-acetylamino)-5-((2S,3R,4S,5S,6R)-3,4,5-triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-4-yl ester

Synonyms:Acetic acid (2R,3R,4S,5R,6R)-3-acetoxy-6-acetoxymethyl-2-(2-{2-[2-(2-azido-ethoxy)-ethoxy]-ethoxy}-acetylamino)-5-((2S,3R,4S,5S,6R)-3,4,5-triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-4-yl ester

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Chemical Property of Acetic acid (2R,3R,4S,5R,6R)-3-acetoxy-6-acetoxymethyl-2-(2-{2-[2-(2-azido-ethoxy)-ethoxy]-ethoxy}-acetylamino)-5-((2S,3R,4S,5S,6R)-3,4,5-triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-4-yl ester

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Technology Process of Acetic acid (2R,3R,4S,5R,6R)-3-acetoxy-6-acetoxymethyl-2-(2-{2-[2-(2-azido-ethoxy)-ethoxy]-ethoxy}-acetylamino)-5-((2S,3R,4S,5S,6R)-3,4,5-triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-4-yl ester

There total 1 articles about Acetic acid (2R,3R,4S,5R,6R)-3-acetoxy-6-acetoxymethyl-2-(2-{2-[2-(2-azido-ethoxy)-ethoxy]-ethoxy}-acetylamino)-5-((2S,3R,4S,5S,6R)-3,4,5-triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-4-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 86520-52-7
2-[2-(2-azidoethoxy)ethoxy]ethanol

: 176167-85-4
Acetic acid (2R,3R,4S,5R,6R)-3-acetoxy-6-acetoxymethyl-2-(2-{2-[2-(2-azido-ethoxy)-ethoxy]-ethoxy}-acetylamino)-5-((2S,3R,4S,5S,6R)-3,4,5-triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-4-yl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / BF₃*Et₂O / CH₂Cl₂ / 6 h / Ambient temperature

2: aq. KOH / ethanol / 6 h / Heating

3: 90 percent / DCC / CH₂Cl₂ / 1 h / Ambient temperature

With potassium hydroxide; boron trifluoride diethyl etherate; dicyclohexyl-carbodiimide; In ethanol; dichloromethane;
DOI:10.1039/cc9960000201

Reference yield:

: 176167-85-4
Acetic acid (2R,3R,4S,5R,6R)-3-acetoxy-6-acetoxymethyl-2-(2-{2-[2-(2-azido-ethoxy)-ethoxy]-ethoxy}-acetylamino)-5-((2S,3R,4S,5S,6R)-3,4,5-triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-4-yl ester

: 176167-91-2
C₄₆H₆₃N₃O₂₆

Guidance literature:: Multi-step reaction with 4 steps

1: H₂ / 10percent Pd/C / methanol / 1 h

2: 65 percent / DIPEA / acetonitrile / 3 h / Ambient temperature

3: 85 percent / DCC / CH₂Cl₂ / 3 h / Ambient temperature

4: 94 percent / TFA / CH₂Cl₂ / 3 h / Ambient temperature

With hydrogen; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; trifluoroacetic acid; palladium on activated charcoal; In methanol; dichloromethane; acetonitrile;
DOI:10.1039/cc9960000201

Reference yield:

: 176167-85-4
Acetic acid (2R,3R,4S,5R,6R)-3-acetoxy-6-acetoxymethyl-2-(2-{2-[2-(2-azido-ethoxy)-ethoxy]-ethoxy}-acetylamino)-5-((2S,3R,4S,5S,6R)-3,4,5-triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-4-yl ester

: 176167-88-7
C₅₀H₇₁N₃O₂₆

Guidance literature:: Multi-step reaction with 3 steps

1: H₂ / 10percent Pd/C / methanol / 1 h

2: 65 percent / DIPEA / acetonitrile / 3 h / Ambient temperature

3: 85 percent / DCC / CH₂Cl₂ / 3 h / Ambient temperature

With hydrogen; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; palladium on activated charcoal; In methanol; dichloromethane; acetonitrile;
DOI:10.1039/cc9960000201