p-octyloxyphenyl 3,4,6-tri-O-acetyl-2-N-phthaloyl-β(1-6)-D-glucosaminyl-1-thio-2,3,4-tri-O-benzyl-β-D-glucopyranoside

Base Information

Chemical Name:p-octyloxyphenyl 3,4,6-tri-O-acetyl-2-N-phthaloyl-β(1-6)-D-glucosaminyl-1-thio-2,3,4-tri-O-benzyl-β-D-glucopyranoside
CAS No.:1242660-05-4
Molecular Formula:C₆₁H₆₉NO₁₅S
Molecular Weight:1088.28
Hs Code.:

Synonyms:p-octyloxyphenyl 3,4,6-tri-O-acetyl-2-N-phthaloyl-β(1-6)-D-glucosaminyl-1-thio-2,3,4-tri-O-benzyl-β-D-glucopyranoside

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Chemical Property of p-octyloxyphenyl 3,4,6-tri-O-acetyl-2-N-phthaloyl-β(1-6)-D-glucosaminyl-1-thio-2,3,4-tri-O-benzyl-β-D-glucopyranoside

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Technology Process of p-octyloxyphenyl 3,4,6-tri-O-acetyl-2-N-phthaloyl-β(1-6)-D-glucosaminyl-1-thio-2,3,4-tri-O-benzyl-β-D-glucopyranoside

There total 1 articles about p-octyloxyphenyl 3,4,6-tri-O-acetyl-2-N-phthaloyl-β(1-6)-D-glucosaminyl-1-thio-2,3,4-tri-O-benzyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1242660-00-9
3,4,6-tri-O-acetyl-2-N-phthaloyl-β(1-6)-D-glucosaminyl-2,3,4-tri-O-benzyl-β-D-glucopyranosyl p-octyloxyphenyl sulfoxide

: 1242660-05-4
p-octyloxyphenyl 3,4,6-tri-O-acetyl-2-N-phthaloyl-β(1-6)-D-glucosaminyl-1-thio-2,3,4-tri-O-benzyl-β-D-glucopyranoside

Guidance literature:: With triphenylphosphine; In tetrachloromethane; acetonitrile; for 2h; Reflux;
DOI:10.1248/cpb.58.758

Reference yield: 76.0%

: 53008-65-4,641635-63-4
methyl 2,3,4-tri-O-benzyl-D-glucopyranoside

: 1242660-05-4
p-octyloxyphenyl 3,4,6-tri-O-acetyl-2-N-phthaloyl-β(1-6)-D-glucosaminyl-1-thio-2,3,4-tri-O-benzyl-β-D-glucopyranoside

: methyl [(3,4,6-tri-O-acetyl-2-N-phthaloyl-D-glucosaminyl)-β(1-6)-2,3,4-tri-O-benzoyl-D-glucopyranosyl]-β(1-6)-2,3,4-tri-O-benzyl-β-D-glucopyranoside

Guidance literature:: With N-iodo-succinimide; trifluorormethanesulfonic acid; In dichloromethane; at -50 ℃; for 0.416667h; Molecular sieve;
DOI:10.1248/cpb.58.758

Reference yield:

: 53008-65-4,641635-63-4
methyl 2,3,4-tri-O-benzyl-D-glucopyranoside

: 1242660-05-4
p-octyloxyphenyl 3,4,6-tri-O-acetyl-2-N-phthaloyl-β(1-6)-D-glucosaminyl-1-thio-2,3,4-tri-O-benzyl-β-D-glucopyranoside

: 1242660-09-8
methyl [(3,4,6-tri-O-acetyl-2-N-phthaloyl-D-glucosaminyl)-β(1-6)-2,3,4-tri-O-benzyl-D-glucopyranosyl]-β(1-6)-2,3,4-tri-O-benzyl-α-D-glucopyranoside

: methyl [(3,4,6-tri-O-acetyl-2-N-phthaloyl-D-glucosaminyl)-β(1-6)-2,3,4-tri-O-benzyl-D-glucopyranosyl]-β(1-6)-2,3,4-tri-O-benzyl-β-D-glucopyranoside

Guidance literature:: With N-iodo-succinimide; trifluorormethanesulfonic acid; In dichloromethane; at -50 ℃; for 1h; optical yield given as %de; Molecular sieve;
DOI:10.1248/cpb.58.758