3,4,6-tri-O-acetyl-2-N-phthaloyl-β(1-6)-D-glucosaminyl-2,3,4-tri-O-benzyl-β-D-glucopyranosyl p-octyloxyphenyl sulfoxide

Base Information

• Chemical Name: 3,4,6-tri-O-acetyl-2-N-phthaloyl-β(1-6)-D-glucosaminyl-2,3,4-tri-O-benzyl-β-D-glucopyranosyl p-octyloxyphenyl sulfoxide
• CAS No.: 1242660-00-9
• Molecular Formula: C₆₁H₆₉NO₁₆S
• Molecular Weight: 1104.28

Synonyms:3,4,6-tri-O-acetyl-2-N-phthaloyl-β(1-6)-D-glucosaminyl-2,3,4-tri-O-benzyl-β-D-glucopyranosyl p-octyloxyphenyl sulfoxide

Chemical Property of 3,4,6-tri-O-acetyl-2-N-phthaloyl-β(1-6)-D-glucosaminyl-2,3,4-tri-O-benzyl-β-D-glucopyranosyl p-octyloxyphenyl sulfoxide

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Technology Process of 3,4,6-tri-O-acetyl-2-N-phthaloyl-β(1-6)-D-glucosaminyl-2,3,4-tri-O-benzyl-β-D-glucopyranosyl p-octyloxyphenyl sulfoxide

There total 1 articles about 3,4,6-tri-O-acetyl-2-N-phthaloyl-β(1-6)-D-glucosaminyl-2,3,4-tri-O-benzyl-β-D-glucopyranosyl p-octyloxyphenyl sulfoxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

p-octyloxyphenyl 2-deoxy-2-phthalimido-3,4,6-tri-O-acetyl-1-thio-β-D-glucopyranoside (916497-81-9) + p-oxtyloxyphenyl 2,3,4-tri-O-benzyl-β-D-glucopyranosyl sulfoxide, → 3,4,6-tri-O-acetyl-2-N-phthaloyl-β(1-6)-D-glucosaminyl-2,3,4-tri-O-benzyl-β-D-glucopyranosyl p-octyloxyphenyl sulfoxide (1242660-00-9)

Guidance literature:

With N-iodo-succinimide; trifluorormethanesulfonic acid; In dichloromethane; at -50 ℃; for 0.25h; Molecular sieve;

DOI:10.1248/cpb.58.758

Reference yield: 82.0%

3,4,6-tri-O-acetyl-2-N-phthaloyl-β(1-6)-D-glucosaminyl-2,3,4-tri-O-benzyl-β-D-glucopyranosyl p-octyloxyphenyl sulfoxide (1242660-00-9) → p-octyloxyphenyl 3,4,6-tri-O-acetyl-2-N-phthaloyl-β(1-6)-D-glucosaminyl-1-thio-2,3,4-tri-O-benzyl-β-D-glucopyranoside (1242660-05-4)

Guidance literature:

With triphenylphosphine; In tetrachloromethane; acetonitrile; for 2h; Reflux;

DOI:10.1248/cpb.58.758

upstream raw materials:

p-octyloxyphenyl 2-deoxy-2-phthalimido-3,4,6-tri-O-acetyl-1-thio-β-D-glucopyranoside

Downstream raw materials:

p-octyloxyphenyl 3,4,6-tri-O-acetyl-2-N-phthaloyl-β(1-6)-D-glucosaminyl-1-thio-2,3,4-tri-O-benzyl-β-D-glucopyranoside

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