Acetic acid benzoylamino-[(E)-3-(4-methoxy-phenyl)-allylsulfanylcarbonyl]-methyl ester

Base Information

Chemical Name:Acetic acid benzoylamino-[(E)-3-(4-methoxy-phenyl)-allylsulfanylcarbonyl]-methyl ester
CAS No.:112654-54-3
Molecular Formula:C₂₁H₂₁NO₅S
Molecular Weight:399.467
Hs Code.:

Synonyms:Acetic acid benzoylamino-[(E)-3-(4-methoxy-phenyl)-allylsulfanylcarbonyl]-methyl ester

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Chemical Property of Acetic acid benzoylamino-[(E)-3-(4-methoxy-phenyl)-allylsulfanylcarbonyl]-methyl ester

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Technology Process of Acetic acid benzoylamino-[(E)-3-(4-methoxy-phenyl)-allylsulfanylcarbonyl]-methyl ester

There total 4 articles about Acetic acid benzoylamino-[(E)-3-(4-methoxy-phenyl)-allylsulfanylcarbonyl]-methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 108-24-7
acetic anhydride

: 112654-53-2
Benzoylamino-hydroxy-thioacetic acid S-[(E)-3-(4-methoxy-phenyl)-allyl] ester

: 112654-54-3
Acetic acid benzoylamino-[(E)-3-(4-methoxy-phenyl)-allylsulfanylcarbonyl]-methyl ester

Guidance literature:: With pyridine; In dichloromethane; for 0.333333h;
DOI:10.1021/jo00239a031

Reference yield:

: 19791-95-8,19791-97-0,16555-77-4
α-hydroxyhippuric acid

: 112654-54-3
Acetic acid benzoylamino-[(E)-3-(4-methoxy-phenyl)-allylsulfanylcarbonyl]-methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 48 percent / dicyclohexylcarbodiimide, 4-(dimethylamino)pyridine / dimethylformamide / 4 h / Ambient temperature

2: 94 percent / pyridine / CH₂Cl₂ / 0.33 h

With pyridine; dmap; dicyclohexyl-carbodiimide; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo00239a031

Reference yield:

: 94607-41-7
(E)-1-(4-methoxyphenyl)-3-chloropropene

: 112654-54-3
Acetic acid benzoylamino-[(E)-3-(4-methoxy-phenyl)-allylsulfanylcarbonyl]-methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) sodium iodide, thiourea, 2.) ethylenediamine / 1.) ethanol, reflux, 2 h, 2.) reflux, 30 min

2: 48 percent / dicyclohexylcarbodiimide, 4-(dimethylamino)pyridine / dimethylformamide / 4 h / Ambient temperature

3: 94 percent / pyridine / CH₂Cl₂ / 0.33 h

With pyridine; dmap; ethylenediamine; thiourea; dicyclohexyl-carbodiimide; sodium iodide; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo00239a031