2-aminohex-5-enyl trityl ether

Base Information

Chemical Name:2-aminohex-5-enyl trityl ether
CAS No.:220254-18-2
Molecular Formula:C₂₅H₂₇NO
Molecular Weight:357.495
Hs Code.:

Synonyms:2-aminohex-5-enyl trityl ether

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Chemical Property of 2-aminohex-5-enyl trityl ether

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Technology Process of 2-aminohex-5-enyl trityl ether

There total 4 articles about 2-aminohex-5-enyl trityl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 220254-17-1
5-Azido-6-(trityloxy)hex-1-ene

: 220254-18-2
2-aminohex-5-enyl trityl ether

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; for 1h; Heating;
DOI:10.1055/s-1999-3681

Reference yield:

: 36842-44-1
hex-5-ene-1,2-diol

: 220254-18-2
2-aminohex-5-enyl trityl ether

Guidance literature:: Multi-step reaction with 3 steps

1: 99 percent / pyridine / 12 h / 45 °C

2: 77 percent / DEAD, PPh₃, (PhO)2P(O)N₃ / tetrahydrofuran / 12 h / Ambient temperature

3: 73 percent / LiAlH₄ / tetrahydrofuran / 1 h / Heating

With pyridine; lithium aluminium tetrahydride; diphenyl phosphoryl azide; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran;
DOI:10.1055/s-1999-3681

Reference yield:

: 76-83-5
trityl chloride

: 220254-18-2
2-aminohex-5-enyl trityl ether

Guidance literature:: Multi-step reaction with 3 steps

1: 99 percent / pyridine / 12 h / 45 °C

2: 77 percent / DEAD, PPh₃, (PhO)2P(O)N₃ / tetrahydrofuran / 12 h / Ambient temperature

3: 73 percent / LiAlH₄ / tetrahydrofuran / 1 h / Heating

With pyridine; lithium aluminium tetrahydride; diphenyl phosphoryl azide; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran;
DOI:10.1055/s-1999-3681