trimethylsilanylmethyl(1-trityloxymethylpent-4-enyl)carbamic acid methyl ester

Base Information

Chemical Name:trimethylsilanylmethyl(1-trityloxymethylpent-4-enyl)carbamic acid methyl ester
CAS No.:375394-17-5
Molecular Formula:C₃₁H₃₉NO₃Si
Molecular Weight:501.741
Hs Code.:

Synonyms:trimethylsilanylmethyl(1-trityloxymethylpent-4-enyl)carbamic acid methyl ester

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Chemical Property of trimethylsilanylmethyl(1-trityloxymethylpent-4-enyl)carbamic acid methyl ester

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Technology Process of trimethylsilanylmethyl(1-trityloxymethylpent-4-enyl)carbamic acid methyl ester

There total 2 articles about trimethylsilanylmethyl(1-trityloxymethylpent-4-enyl)carbamic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 79-22-1
methyl chloroformate

: 375394-16-4
2-((trimethylsilanyl)methylamino)hex-5-enyl trityl ether

: 375394-17-5
trimethylsilanylmethyl(1-trityloxymethylpent-4-enyl)carbamic acid methyl ester

Guidance literature:: With sodium hydroxide; In water; at 0 ℃; for 0.5h;
DOI:10.1021/jo010144b

Reference yield:

: 220254-18-2
2-aminohex-5-enyl trityl ether

: 375394-17-5
trimethylsilanylmethyl(1-trityloxymethylpent-4-enyl)carbamic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 60 percent / KI; Na₂CO₃ / acetonitrile / 12 h / 83 °C

2: 96 percent / NaOH / H₂O; various solvent(s) / 0.5 h / 0 °C

With sodium hydroxide; sodium carbonate; potassium iodide; In water; acetonitrile;
DOI:10.1021/jo010144b