(S)-tert-butyl (1-(1H-benzo[d][1,2,3]triazol-1-yl)-1-oxo-3-(1-tosyl-1H-imidazol-4-yl)propan-2-yl)carbamate

Base Information

• Chemical Name: (S)-tert-butyl (1-(1H-benzo[d][1,2,3]triazol-1-yl)-1-oxo-3-(1-tosyl-1H-imidazol-4-yl)propan-2-yl)carbamate
• CAS No.: 1381762-41-9
• Molecular Formula: C₂₄H₂₆N₆O₅S
• Molecular Weight: 510.574

Synonyms:(S)-tert-butyl (1-(1H-benzo[d][1,2,3]triazol-1-yl)-1-oxo-3-(1-tosyl-1H-imidazol-4-yl)propan-2-yl)carbamate

Chemical Property of (S)-tert-butyl (1-(1H-benzo[d][1,2,3]triazol-1-yl)-1-oxo-3-(1-tosyl-1H-imidazol-4-yl)propan-2-yl)carbamate

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of (S)-tert-butyl (1-(1H-benzo[d][1,2,3]triazol-1-yl)-1-oxo-3-(1-tosyl-1H-imidazol-4-yl)propan-2-yl)carbamate

There total 1 articles about (S)-tert-butyl (1-(1H-benzo[d][1,2,3]triazol-1-yl)-1-oxo-3-(1-tosyl-1H-imidazol-4-yl)propan-2-yl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

1-(methanesulfonyl)-1H-1,2,3-benzotriazole (37073-15-7) + Boc-His(Tos)-OH (35899-43-5) → (S)-tert-butyl (1-(1H-benzo[d][1,2,3]triazol-1-yl)-1-oxo-3-(1-tosyl-1H-imidazol-4-yl)propan-2-yl)carbamate (1381762-41-9)

Guidance literature:

With triethylamine; In N,N-dimethyl-formamide; at 50 ℃; for 0.5h; Irradiation;

DOI:10.1002/psc.2483

Reference yield: 92.0%

L-alanin (56-41-7,25191-17-7,18875-37-1) + (S)-tert-butyl (1-(1H-benzo[d][1,2,3]triazol-1-yl)-1-oxo-3-(1-tosyl-1H-imidazol-4-yl)propan-2-yl)carbamate (1381762-41-9) → 2-((S)-2-(tert-butoxycarbonylamino)-3-(1-tosyl-1H-imidazol-4-yl)propanamido)propanoic acid (1420199-44-5)

Guidance literature:

With triethylamine; In water; at 20 ℃;

DOI:10.1002/psc.2483

Reference yield: 92.0%

N-(3-aminopropyl)imidazole (1342064-59-8) + (S)-tert-butyl (1-(1H-benzo[d][1,2,3]triazol-1-yl)-1-oxo-3-(1-tosyl-1H-imidazol-4-yl)propan-2-yl)carbamate (1381762-41-9) → (S)-tert-butyl (1-((3-(1H-imidazol-1-yl)propyl)amino)-1-oxo-3-(1-tosyl-1H-imidazol-4-yl)propan-2-yl)carbamate

Guidance literature:

With triethylamine; In tetrahydrofuran; at 20 ℃; for 3h;

DOI:10.1002/psc.2483

upstream raw materials:

1-(methanesulfonyl)-1H-1,2,3-benzotriazole

Boc-His(Tos)-OH

Downstream raw materials:

(S)-4-ethylphenyl 2-(tert-butoxycarbonylamino)-3-(1-tosyl-1H-imidazol-4-yl)propanoate

(S)-naphthalen-2-yl 2-(tert-butoxycarbonylamino)-3-(1-tosyl-1H-imidazol-4-yl)propanoate

(S)-S-benzyl 2-((tert-butoxycarbonyl)amino)-3-(1-tosyl-1Himidazol-4-yl)propanethioate

(S)-methyl 2-((2-((tert-butoxycarbonyl)amino)-3-(1-tosyl-1H-imidazol-4-yl)propanoyl)thio)acetate

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